GCMS analysis results for sample AE01045, March 2002

NYC 9/11 Public Portal Document

Data File : C:\MSDCHEM\l\DATA\022802\01045.D Vial: 10 Acq On : 28 Feb 2002 6:21 pm Operator: McLean . Sample : GC MS SCAN 2/27 Inst Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\1\5973N\5080202.M (RTE Integrator) Title : Quantitation For Method 508gcscan Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 1 Cyclopentasiloxane, decamet... Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

12.08 2.69 ug/L 860517 Naphthalene-d8 13.05

Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 91 2 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 59 3 Phenethylamine, N-methyl-.beta. ,... 399 C18H37NO3Si3 010538-85-9 47 4 N- (Trifluoroacetyl)-N,0,0‘,0‘‘-t... 553 C22H42F3NO4Si4 000000-00-0 38 Abundance Scan 993 (12.083 min): 01045.D (-) m/z 73.10 ’ 100.00% 73

5000 267 355

11.80 12.00 12.20 12.40 45 108 133154 193,223 lt 11 293 323 _ m/z 267.00 45.28% 0- • i ’ 77* i ■ 1 ■ ' /‘* “ । * ‘ • ■■ r 17 TITm m/z-> 50 100 150 200 250 300 350 Abundance #313065: Cyclopentasiloxane, decamethyl- 73

5000 267 0 11.80 12.00 12.20 12.40 355 m/z 355.10 38.29% 45 96 133 165 193 11,223 247,1 293 323 . i 0 nr m/z-> 50 100 150 200 250 300 350 Abundance #313068: Cvclopentasiloxane, decamethyl- 73

T 355 11.80 12.00 12.20 12.40 267 m/z 356.10 12.82% 5000

45

m/z-> 0 I 50 100 150 —7 —2344 200 250 300 350 Abundance #331718: Phenethylamine, N-methyl-.beta.,3,4-tris(trimethy... 73 ‘ I‘14‘W 11.80 12.00 12.20 12.40 m/z 268.00 11.37%

5000 355

44

93 116 147 193 220 267 294 384 Im/z-> 0 — I -"1 > n IT-r-i •> 100 150 200 250 " r 300 1-* 1 ' I ■ ' 1 1 i 1 ' 11.80 12.00 12.20 12.40 50 350

01045.D 5080202.M Wed Mar 13 11:01:03 2002 Page 3

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