GCMS analysis results for sample AE04241, Mar 2002

NYC 9/11 Public Portal Document Data File : C:\MSDCHEM\l\DATA\022802\04241.D Vial: 12 Acq On : 28 Feb 2002 7:59 pm Operator: McLean Sample : GC MS SCAN 2/27 Inst Instrumen • Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\l\5973N\5080202.M (RTE Integrator) Title : Quantitation For Method 508gcscan Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 1 Cyclopentasiloxane, decamet... Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

12.08 1.87 ug/L 621729 Naphthalene-d8 13.05

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 91 2 Phenethylamine, N-methyl-.beta.,... 399 C18H37NO3Si3 010538-85-9 47 3 N-(Trifluoroacetyl)-N,0,0',0'’-t... 553 C22H42F3NO4Si4 000000-00-0 38 4 Benzeneacetic acid, .alpha.,3,4-... 472 C20H40O5Si4 037148-65-5 38 Abundance Scan 993 (12.083 min): 04241 .D (-) m/ z 73.10 100.00% 73

5000 267 355

11.80 12.00 12.20 12.40 108 154 193223 . 323 m/z 267.00 46.83% 0 — —IPTTt m/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #313068: Cyclopentasiloxane, decamethyl- 73

355 267 5000 ''' i ■ ■ ■ ■ i ' i ■ ■ ■ ■ i ■ ■' ■ 11.80 12.00 12.20 12.40 m/z 355.10 38.26%

,1... 300323.350 400 450 500 550 I 0 m/z-> 50 100 150 200 250 Abundance #331718: Phenethylamine, N-methyi-.beta.,3,4-tris(trimethy... 73

11 1 1 ‘ i '1 I T 11.80 12.00 12.20 12.40 5000 m/z 356.10 12.84% 355 44

m/z-> 0- 50 + -nm” 1’ l 116147 193 237267 309 '''I 1*4" 100 150 200 250 300 350 400 450 500 550 384

Abundance #377151: N-(Trifluoroacetyl)-N,O>O',O''-tetrakis(trimethyl... 73 ■ • i ■ • 1.. 11.80 12.00 12.20 12.40 m/z 268.00 10.21% 355 5000

0 44 116 147 193 236267 538 ••।•••>। m/z-> 50 100 150 200 250 300 350 400 450 500 550 11.80 12.00 12.20 12.40

04241.D 5080202.M Wed Mar 13 11:10:42 2002 Page 3

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