NYC-WTC_000052539
GCMS analysis report for sample AE04241 identifying unknown compounds and DDD in March 2002.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗Document / 9 pages
GCMS analysis results for sample AE04243, Mar 2002
Machine-extracted title · confidence 100%GCMS analysis report for sample AE04243 identifying unknown compounds and DDD in March 2002.
NYC-WTC_000052557–000052565Folder label: “GCMS X 1/15/02 A 2/28/02”
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NYC 9/11 Public Portal Document
•Data File : C:\MSDCHEM\l\DATA\022802\04243.D Vial: 11 Acq On : 28 Feb 2002 7:10 pm Operator: McLean Sample : GC MS SCAN 2/27 Inst : Instrumen Mise : Multiplr; 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1\5973N\5080202.M (RTE Integrator) Title : Quantitation For Method 508gcscan Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 1 Cyclopentasiloxane, decamet... Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T.
12.08 5.07 ug/L 1640910 Naphthalene-d8 13.05
Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 62 2 Benzoic acid, 2-[ (trimethylsilyl— 282 C13H2203Si2 003789-85-3 47 3 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 46 4 N-(Trifluoroacetyl)-N, 0,0',0"-t... 553 C22H42F3NO4Si4 000000-00-0 32 Abundance Scan 993 (12.083 min): 04243.D (-) m/z 73.10 100.00% 73
5000 267 355 mIImer ’111 " 11' ‘ 11.80 12.00 12.20 12.40 45 108 133154 _1?3 223 ,L 293 323 . m/z 267.00 47.45% 0- — TPTT 1 “t m/z-> 50 100 150 200 250 300 350 Abundance #313068: Cyclopentasiloxane, decamethyl- 73
355 5000 267 p 11.80 12.00 12.20 12.40 m/z355.10 37.17%
0- 45 I__ TL 207 *P*1i [ 1-T 323 | I m/z-> 50 100 150 200 250 300 350 Abundance #227687: Benzoic acid, 2-[(Mmethylsilyl)oxy]-, trimethyl... 73 267
1180 12.00 12.20 12.40” 5000 m/z 356.10 13.12%
135 0- 47 1 'I +** ,9,115.1+ 193— -— — 233r . —— m/z-> 50 100 150 200 250 300 350 Abundance #313065: Cyclopentasiloxane, decamethyl- 73 11.80 12.00 12.20 1240” m/z 268.00 10.23%
5000 267 355 45 0 20 11, 96 133 165 193,.223 247,1 293 323 TTTI ’ • i •411) ■ • m/z-> 50 100 150 200 250 300 350 ' 11.80 12.00 12.20 12.40
04243.D 5080202.M Wed Mar 13 11:13:02 2002 Page 3
NYC-WTC_000052564
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NYC-WTC_000052564Source: NYC Law Department, mirrored locally
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NYC-WTC_000052566
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machine-extracted · confidence unavailable · Check page ↗Filed elsewhere
NYC-WTC_000005992
Technical comment regarding low recovery rates in GCMS scan of sample AE03016, indicating a decision to reextract and reanalyze the specimen.
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machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000006001
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1 shared topics · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000005925
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1 shared topics · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000038431
Quantitation report listing response data for deuterated internal standards and surrogates from a March 14, 2002 analysis.
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machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000038440
Quantitation report listing response data for deuterated internal standards and surrogates from a March 14, 2002 analysis.
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machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000011192
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