GCMS quantitation results for sample AE03440, March 2002

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Data- File C:\MSDCHEM\l\DATA\022802\03440.D Vial: 27 * Acq On 1 Mar 2002 9:53 am Operator: McLean Sample : Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\1\5973N\5080202.M (RTE Integrator) Title : Quantitation For Method 508gcscan Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 1 Cyclopentasiloxane, decamet... Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

12.08 1.46 ug/L 502725 Naphthalene-d8 13.05

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 53 2 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 46 3 3,4-Dihydroxybenzyl alcohol,tris... 356 C16H3203Si3 068595-79-9 40 4 Benzoic acid, 2-[(trimethylsilyl... 282 C13H22O3Si2 003789-85-3 37 Abundance Scan 993 (12.083 min): 03440.D (-) m/z 73.10 100.00% 73

5000 267 355

45 11.80 12 00 12.20 12.40 I 133154 1?3 223 323 1 [ m/z 267.00 46.44% 0- ‘I 1*1* 11 1)’ 1 1I ■— I ——r m/z-> 50 100 150 200 250 300 350 Abundance #313068: Cyclopentasiloxane, decamethyl- 73

355 267 5000 11.80 12*00 1Z20 1240 * m/z 355.10 37.27%

45 207 323 , m/z-> 0- • ‘ | 50 l । ' ‘ ________ ' 100 l ' 150 • ■ i • ■ ' 200 —P ” i "‘ 250 r 300T"■ r 4 350 Abundance #313065: Cyclopentasiloxane, decamethyl- 73

"UF T 11 T 11.80 12.00 12.20 12.40 m/z 356.10 12.13% 5000 267 355 45 0- ■ ■ 4— 11 96 133 1654123 223 2474 . 293 323 • 1 ' T11 1 ” L ‘ m/z-> 50 100 150 200 250 300 350 Abundance #302823: 3,4-Dihydroxybenzyl alcohol,tris(trimethylsily!)- 73 T T 11 T 11.80 12.00 12.20 12.40 m/z 268.00 10.01%

267 5000 179 356 45 147 15 J ... 103 k 209 237 1. 1—1312 0 11r 1 * r y Tr 1. fi — m/z—> 50 100 150 200 250 300 350 11.80 12.00 12.20 12.40

03440.D 5080202.M Wed Mar 13 06:51:09 2002 Page 3

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