GCMS blank analysis report for sample AE01002, Mar 2002

NYC 9/11 Public Portal Document

Data File : C:\MSDCHEM\l\DATA\022802\0226LB.D Vial: 6 Acq On : 28 Feb 2002 3:05 pm Operator: McLean Sample : GC MS SCAN 2/27 Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\1\5973N\5080202.M (RTE Integrator) Title : Quantitation For Method 508gcscan Library : C:\DATABASE\WILEY7N.L

Peak Number 1 Cyclopentasiloxane, decamet... Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

12.08 1.79 ug/L 565427 Naphthalene-d8 13.05

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 91 2 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 58 3 Benzoic acid, 2-[(trimethylsilyl ... 282 C13H2203Si2 003789-85-3 47 4 Phenethylamine, N-methyl-.beta. ,... 399 C18H37NO3Si3 010538-85-9 38 Abundance Scan 993 (12.083 min): 0226LB.D (-) m/ z 73.10 100.00% 73

5000 267 355 ----- 45 11.80 12.00 12.20 12.40 133 154 I?3 223 । 323 m/z 267.00 44.41% 01 — । Mr—et" A |". ridrf 14 rP—+T" m/z-> 50 100 150 200 250 ;300 350 Abundance #313065: Cyclopentasiloxane, decamethyl- 73

5000 267 PPP ■ i ' • 11.80 12.00 12.20 12.40 355 m/z 355.10 37.13% 45 0 26—14 96 133 165,193 223 247 l 293 323 1 ' i 1 [ 1 * 1 1 m/z-> 50 100 150 200 250 300 350 Abundance #313068: Cyclopentasiloxane, decamethyl- 73 — TTrr 355 11.80 12.00 12.20 12.40 267 m/z 356.10 14.34% 5000

45 323 , | 0 207 ii ,1.1” m/z-> 50 100 150 200 250 300 350 Abundance #227687: Benzoic acid, 2-[(trimethylsilyl)oxy]-, trimethyl... 73 267 T 11.80 12.00 12.20 12.40 m/z 268.00 12.27%

5000

135 193

m/z-> 0 47 II 50 1, 92,115,4 .. 133 100 150 200 233 250 300 350 11.80 12.00 12.20 12.40

0226LB.D 5080202.M Wed Mar 13 11:08:02 2002 Page 3

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