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GCMS analysis results for sample AE01044, March 2002

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Laboratory report documenting GCMS analysis of sample AE01044 conducted on March 14, 2002.

NYC-WTC_000052607–000052613

Folder label: “GCMS X 1/15/02 A 2/28/02

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NYC 9/11 Public Portal Document Data File : C:\MSDCHEM\1\DATA\022802\01044.D Vial: 7 Acq On : 28 Feb 2002 3:54 pm Operator: McLean Sample : GC MS SCAN 2/27 Inst : Instrumen * Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\l\5973N\5080202.M (RTE Integrator) Title : Quantitation For Method 508gcscan Library : C:\DATABASE\WILEY7N.L

Peak Number 1 Cyclopentasiloxane, decamet... Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

12.08 1.37 ug/L 394507 Naphthalene-d8 13.05

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 64 2 Phenethylamine, N-methyl-.beta.,... 399 C18H37NO3Si3 010538-85-9 47 3 N-(Trifluoroacetyl)-N, 0,0',O''-t... 553 C22H42F3NO4Si4 000000-00-0 43 4 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 38 Abundance Scan 993 (12.083 min): 01044.D (-) m/z 73.10 100.00% 73

5000 267 355 —IPPr V............. 11.80 12.00 12.20 12.40 154 193223 , 323 m/z 267.00 47.47% 0 - m/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #313068: Cyclopentasiloxane, decamethyl- 73

355 267 5000 T 11.80 12.00 12.20 12.40 m/z 355.10 40.30%'

01- 207 . Tr 323 m/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #331718: Phenethylamine, N-methyl-.beta.,3,4-tris(trimethy... 73 ----- 11.80 12.00 12.20 12.40 5000 m/z 356.10 12.24% 355 44 a 4 116147 193 237267 309 384 0 m/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #377151: N-(Trifluoroacetyl)-N1O>O',O"-tetrakis(trimethyl... 73 T 1‘I T 11.80 12.00 12.20 12.40 m/z 268.00 10.86% 355 5000

44 > 116147,193,236267 , 0 TTTT 538 m/z-> 50 100 150 200 250 300 350 400 450 500 550 11.80 12.00 12.20 12.40

01044.D 5080202.M Wed Mar 13 10:59:58 2002 Page 3

NYC-WTC_000052612

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NYC-WTC_000052612Source: NYC Law Department, mirrored locally

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