GCMS quantitation results for sample AE03438, March 2002

NYC 9/11 Public Portal Document

Data File C:\MSDCHEM\l\DATA\022802\03438.D Vial: 25 . Acq On 1 Mar 2002 8:15 am Operator: McLean Sample : Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\1\5973N\5080202.M (RTE Integrator) Title : Quantitation For Method 508gcscan Library : C:\DATABASE\WILEY7N.L ********************************* ************************************ Peak Number 1 Cyclopentasiloxane, decamet... Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

12.08 1.23 ug/L 393853 Naphthalene-d8 13.05

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 78 2 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 49 3 Phenethylamine, N-methyl-.beta.,... 399 C18H37NO3Si3 010538-85-9 43 4 Benzeneacetic acid,' .alpha.,4-bi... 384 C17H3204Si3 037148-64-4 38 Abundance Scan 993 (12.083 mln): 03438.D (-) m/z 73.10 100.00% 73

5000 267 355 —In- i । i > r i | / 11-1 | i > . . | l . . I

11.80 12.0012.2012.40 45 133154 1?3 237,! 323 - m/z 267.00 48.29% 0- , TPIIT 11 —I t ■ i —r 1 i ■ m/z-> 50 100 150 200 250 300 350 Abundance #313065: Cyclopentasiloxane, decamethyl- 73

5000' 267 —11 .. .............. 11.80 12.00 12.20 12.40 355 m/z 355.10 36.81% 45 0- — 96 , 133 165 123 223 247,1 —— 293 323 m/z-> 50 100 150 200 250 300 350 Abundance #313068: Cyclopentasiloxane, decamethyl- 73 —................ ■ ■ 11 • • 355 11.80 12.00 12.20 12.40 267 m/z 356.10 15.89% 5000

45 207 323 0- - ■ f — 1 11+ I 4— m/z-> 50 100 ' ‘ 150 ' 200 250 300 350 Abundance #331718: Phenethylamine, N-methyl-.beta.,3,4-tris(trlmethy... 7 T T T T 11.80 12.00 12.20 12.40 m/z 268.00 11.94%

5000 355

44

93 116 147 193 220 384 0 —iI TTTvr 267 294 ■ i • ■ • • l • ‘ * i T T m/z—> 50 100 150 200 250 300 350 11.80 12.00 12.20 12.40

03438.D 5080202.M Wed Mar 13 06:48:41 2002 Page 3

NYC-WTC_000038429