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GCMS quantitation results for sample AE03471, March 2002

Machine-extracted title · confidence 95%

Quantitation report listing response data for deuterated internal standards and surrogates from a March 14, 2002 analysis.

NYC-WTC_000038458–000038464

Folder label: “GCMS X 2/26/02 A 2/28/02

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NYC 9/11 Public Portal Document

Data File C:\MSDCHEM\l\DATA\022802\03471.D Vial: 20 Acq On 1 Mar 2002 4:08 am Operator: McLean * Sample Inst ; Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\1\5973N\5080202.M (RTE Integrator) Title : Quantitation For Method 508gcscan Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 1 Cyclopentasiloxane, decamet... Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

12.08 1.41 ug/L 454673 Naphthalene-d8 13.05

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 47 2 Benzeneethanamine, N-[(pentafluo... 563 C24H34F5NO3Si3 055429-13-5 43 3 Phenethylamine, N-methyl-.beta.,... 399 C18H37NO3Si3 010538-85-9 43 . 4 N-(Trifluoroacetyl)-N, 0,0',011-t... 553 C22H42F3NO4S14 000000-00-0 38 Abundance Scan 993 (12.083 mln): 03471.D (-) m/z 73.10100.00% 73

5000 267 355 . . । . i i । । . 11.80 12.00 12.20 12.40 0- - 103;TTrfp 154 193223 , 323 (■ 1 ■ PI. 1111 ■ J • ‘ • i • * ' ‘ I > ‘ m/z 267.00 47.90% miz-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #313068: Cyclopentasiloxane, decamethyl- 73

355 267 5000 1111 ■1 > > i /•> • i ■‘ • p ■ ■ • 11.80 12.00 12.20 12.40 m/z 355.10 38.08%

207 * 323. 323, 0- — ‘ 1182127 Teme miz—> 50 100 150 200 250 300 350 400 450 500 550 Abundance #378300: Benzeneethanamine, N-K(pentafluoropheny!)methylen... 73 355

11.80 12.00 1220 1240 m/z356.10 13.08% 5000

m/z—> 0- 4 , 100117147177207 50 251281 386 429458 548 1 i ri । । i i । । 'I i-1 i j i i ri '| r i 150 200 250 300 350 400 450 500 550 Abundance #331718: Phenethylamine, N-methyl-.beta.,3,4-tris(trimethy... 73 — i'1 ‘11 11.80 12.00 12.20 12.40 m/z 268.00 11.29%

5000 355

44

0 + 116147.193.237267.30%. IIITTIIT 384 ‘ 111’11 rr-n-p-T -PI miz—> 50 100 150 200 250 300 350 400 450 500 550 11,80 12.00 12.20 12.40

03471.D 5080202.M Wed Mar 13 06:54:46 2002 Page 3

NYC-WTC_000038463

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NYC-WTC_000038463Source: NYC Law Department, mirrored locally

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