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GCMS analysis results for sample AE01045, March 2002

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AE01045 conducted on March 14, 2002.

NYC-WTC_000052620–000052629

Folder label: “GCMS X 1/15/02 A 2/28/02

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Scanned page image, NYC-WTC_000052628
OCR text

OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Data File : C:\MSDCHEM\1\DATA\022802\01045.D Vial: 10 Acq On : 28 Feb 2002 6:21 pm Operator: McLean . Sample : GC MS SCAN 2/27 Inst Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\l\5973N\5080202.M (RTE Integrator) Title : Quantitation For Method 508gcscan Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 2 Sulfur, mol. (S8) (CAS) $$ ... Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

26.03 1.01 ug/L 353990 Phenanthrene-dl0 22.52

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Sulfur, mol. (S8) (CAS) $$ OCTA-... 256 S8 010544-50-0 95 2 Cyclic octaatomic sulfur $$ Sulf... 256 S8 010544-50-0 94 3 Sulfur, mol. (S8) (CAS) $$ OCTA-... 256 S8 010544-50-0 94 4 Sulfur, mol. (S8) (CAS) $$ OCTA-... 256 S8 010544-50-0 91 Abundance Scan 2531 (26.033 min): 01045.D (-) m/z 64.00 100.00% 64

5000 128 160 256 J) 96 192 T T 25.80 26.00 26.20 26.40

m/z--> 01] i । ' > | i mTr 1 111 ■ ■ 124. 1 i1''' 11 20 40 60 80 100 120 140 160 180 200 220 240 260 I ' ' 11' ■ ■ i ■' m/z 127.90 34.34%

Abundance #195803: Sulfur, mol. (S8) (CAS) $$ OCTA-SULFUR S$ S8 $S S... 64

5000 28 L ‘111 256 25.80 26.00 26.20 26.40 160 m/z 255.80 28.36% 128 192 96

m/z-> 0 20 -44— 40 60 '11 • ■ i ■' ■' 11 1 1 ' 1 ' * 80 100 120 140 160 180 200 220 240 260 I_______ ’1'' i ■' 224 || '' gi > । 11 । । । f> FTTIn

Abundance #195805: Cyclic octaatomic sulfur $$ Sulfur, mol. (S8) $$ ... 64 256 "‘ i 25.80 26.00 26.20 26.40 128 160 m/z 159.90 23.78% 5000 192

32 96 224

0 ......... 1 rTrrTr | i •' •' i m-TT — m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 Abundance #195807: Sulfur, mol. (S8) (CAS) $$ OCTA-SULFUR $$ S8 $$ S... -- 64 • ■ I1 25.80 26.00 26.20 26.40 m/z 96.00 18.59%

5000 128 256 160 96 192 34 48 I 80 — 224 — 0- i' 11’1 r1 > ‘It t' ’111 ’ i'' ■11 m/z—> 20 40 60 80 100 120 140 160 180 200 220 240 260 25.80 26.00 26.20 26.40

01045.D 5080202.M Wed Mar 13 11:01:04 2002 Page 4

NYC-WTC_000052628

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NYC-WTC_000052628Source: NYC Law Department, mirrored locally

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