Laboratory report showing GCMS analysis of sample AE00468 with surrogate recovery data on January 18, 2002.
NYC-WTC_000051318–000051335Folder label: “GCMS X 1/8/02 A 1/10/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Data File : C: \MSDCHEM\1\5973N\02JAN10\00468.D Vial: 5 Acq On 10 Jan 2002 6:07 pm Operator: Sample : 508 scan ext 1/8 Inst : Instrumen Mise : January 10, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P
Quant Method : C:\MSDCHEM\1... \SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L
Peak Number 10 Sulfur, mol. (S8) (CAS) $$ ... Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 26.14 84.90 ug/L 46345700 Phenanthrene-dl0 22.63 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Sulfur, mol. (S8) (CAS) $$ OCTA-... 256 S8 010544-50-0 97 2 Sulfur, mol. (S8) (CAS) $$ OCTA-... 256 S8 010544-50-0 97 3 Cyclic octaatomic sulfur 256 S8 010544-50-0 91 4 Sulfur, mol. (S8) (CAS) $$ OCTA-... 256 S8 010544-50-0 91 Abundance Scan 1994 (26.139 min): 00468. D (-) m/ z 64.00 100.00% 64
5000 128 256 160 96 192
miz-> 01 40 44 I 76 ■ ■ ......... r*r-r-n-p-r
60 80 100 120 .1 140 160 180 200 220 240 L ■ ■ 224 i ■ ■ ■ ■ i 1 ■ —I 260 25.80 26.00 26.20 26.40 m/z 127.90 46.07% Abundance #195806: Sulfur, mol. (S8) (CAS) $$ OCTA-SULFUR $$ S8 $$ S... 64 256
160 128 5000
0t 34 i ■ ' ' ■ i I 1 ' 1 I ' ' 96
1 192
1 ' ' ' 1 1 1 224 m/z 7 1 ' 1 1 ' 1 1 I ' 1 ' 25.80 26.00 26.20 26.40 I 1 ▼ 1 "I I 1 1 1 I 1
44.92%
*n/z—> 40 60 80 100 120 140 160 180 200 220 240 260 Abundance #195807: Sulfur, mol. (S8) (CAS) $$ OCTA-SULFUR $$ S8 $$ S... 64
25.80 26.00 26.20 26.40 5000 m/z 159.90 33.94% 128 256 / 96 160 192 0t 34 48 ' ' 1 1 1 ' 1 1 ‘‘I’’ 1......... I, . ....... 1,11,224., ..1/, rn/z--> 40 60 80 100 120 140 160 180 200 220 240 260 Abundance #195804: Cyclic octaatomic sulfur 64 25.80 26.00 26.20 26.40 m/z 95.90 21.13% 5000
7s 96 128 160 192 256 0 34 -r-r-j-r-r . | k, 11... i............ ........................i-.... 1 ' 224 .. , I ' ' 1 1 I ' ' ' 1 I ' m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 25.80 26.00 26.20 26.40
00468.D SCAN508.M Fri Jan 11 10:08:44 2002 Page 12
NYC-WTC_000051333
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NYC-WTC_000051740
GCMS analysis log for sample AE00560 showing surrogate recovery and unknown compounds detected on January 17, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000050774
Laboratory report listing unknown compounds and surrogate recovery for sample AE00106 analyzed on February 7, 2002.
1 shared topics · Same agency, volume and box · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000051586
Laboratory report showing GCMS analysis results for sample AE00613 conducted on February 1, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000050912
Laboratory record documenting GCMS surrogate recovery data for sample AE00281 analyzed on January 10, 2002.
1 shared topics · Same agency, volume and box · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000052291
Laboratory report detailing GCMS scan results for sample AE00844, including detection of unknown compounds and surrogate recovery data.
1 shared topics · Same agency, volume and box · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000052251
Laboratory report showing GCMS analysis of sample AE00842 including surrogate recovery and unknown compounds.
1 shared topics · Same agency, volume and box · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000052311
Laboratory report detailing GCMS scan results for sample AE00841, including detection of unknown compounds and surrogate recovery data.
1 shared topics · Same agency, volume and box · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000050893
Laboratory record documenting GCMS surrogate recovery data for sample AE00280 analyzed on January 10, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000050838
Quality control report for GCMS analysis of sample AE00277 showing surrogate recovery data from January 10, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000051549
Laboratory report showing GCMS analysis results for sample AE00556 conducted on February 1, 2002.
1 shared topics · Same agency, volume and box · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000050754
Laboratory report listing unknown compounds and surrogate recovery for sample AE00108 analyzed on February 7, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000003543
Laboratory report documenting GCMS analysis of sample AE01141 conducted on February 27, 2002.
1 shared non-person entities · 1 shared topics · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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NYC-WTC_000051152
Administrative record from DEP Box 28 documenting GCMS activities at the World Trade Center site in January 2002.
Filed in the same folder
NYC-WTC_000051153
Document header page containing identification codes and metadata for GCMS files processed in early January 2002.
Filed in the same folder
NYC-WTC_000051156
Laboratory report detailing GCMS analysis of sample AE00327 for volatile organic compounds on January 10-11, 2002.
Filed in the same folder
NYC-WTC_000051165
Laboratory report showing GCMS analysis of reference standards used for calibration during January 10-11, 2002 testing.
Filed in the same folder
NYC-WTC_000051179
Laboratory report documenting GCMS blank analysis to verify system cleanliness during January 10-11, 2002 testing.
Filed in the same folder