GCMS analysis results for sample AD28861, Dec 17 2001

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GCMS report for sample AD28861 showing detection of unknown compounds and surrogate recovery data.

NYC-WTC_000018830–000018848

Folder label: “GCMS X 12/17/01 A 12/22 - 12/23/01”

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NYC 9/11 Public Portal Document

Library Search Compound Report • Data File : C:\MSDCHEM\l\5973N\02FEB01\28860.D Vial: 3 Acq On : 1 Feb 2002 12:14 pm Operator: Sample : 508 scan Inst : Instrumen Mise : February 1, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 12 Sulfur, mol. (S8) (CAS) $$ ... Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 26.13 64.79 ug/L 47518700 Phenanthrene-dl0 22.65 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Sulfur, mol. (S8) (CAS) $$ OCTA-... 256 S8 010544-50-0 97 2 Sulfur, mol. (S8) (CAS) $$ OCTA-... 256 S8 010544-50-0 94 3 Sulfur, mol. (S8) (CAS) $$ OCTA-... 256 S8 010544-50-0 91 4 Cyclic octaatomic sulfur 256 S8 010544-50-0 91 Abundance Scan 1993 (26.128 min): 28860.D (-) m/z 64.00 100.00% 64

128 256 5000 160 96 192 1 1 ! 1 ' 1 1 I ‘ ‘ ‘ *1 1 ‘1 1 | ' 1 1 ' 1 25.80 26.00 26.20 26.40

miz-> 0- 44 J 76 ' FTTpi‘ »«l • > 40 60 80 PPP— —PP- 224 1 i • ■ ■ ■ i ‘ 100 120 140 160 180 200 220 240 260 • i ■ ■ 1ur m/z 127.90 49.83% Abundance #195806: Sulfur, mol. (S8) (CAS) $$ OCTA-SULFUR $$ S8 $$ 8... 64 256

160 128 5000 ■ ■ i ■ ‘ ■ i ■ ■ ■ i i ■ • ‘ ■ i ‘ ■ i 25.80 26.00 26.20 26.40 96 192 m/z 255.80 47.79% 224 0- 34 I • ■ ■ । • i ■ ■ ■ ■ i ■ 1 11' 1 ' 1 1 1 -ieephnaipi 260 n/z-> 40 60 80 100 120 140 160 180 200 220 240 Abundance #195807: Sulfur, mol. (S8) (CAS) $$ OCTA-SULFUR $$ S8 $$ S... 64 25.80 26.00 26.20 26.40 5000 m/z 159.90 36.11% 128 256 96 160 192

m/z—> 34 48 OVr ■ ■ i • ' ‘ ‘ i | 40 60 • •»i > • 80 i ■ • ■ ■ i ■ । H 100 120 140 160 180 200 220 240 260 — 224 .... ... ■ ■ i 1 ■ ■ 1 i ■ • ■ I' ■

Abundance #195802: Sulfur, mol. (S8) (CAS) $$ OCTA-SULFUR $$ S8 $$ S... 64 25.80 26.00 26.20 26.40 m/z 95.90 22.64%

5000

128 256

/z—> 0-34, 40 60 L7980— 100 120 140 160 180 200 220 240 260 96 1 i ■ ■ • ■ i ■ 160 192 ■ i ■ ■ ■ ■ 1'' • • ■ i • ■ 224 i ■ • 1 1 1 1 ■ ‘ ■ i ■ ' ■ ‘ i ■ ■ ‘ i I 1 '* 1 1 I 25.80 26.00 26.20 26.40 1 1 1 I

28860.D SCAN508.M Mon Feb 04 08:41:06 2002 Page 14

NYC-WTC_000018847

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NYC-WTC_000018847Source: NYC Law Department, mirrored locally

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GCMS analysis results for sample AD31676, Jan 2002 · Box DEP Box 28

NYC-WTC_000050317

Laboratory report for sample AD31676 documenting detection of unknown compounds and surrogate recovery on January 25, 2002.

1 shared non-person entities · 1 shared topics · similarity 0.998