Laboratory report showing GCMS analysis of sample AE00468 with surrogate recovery data on January 18, 2002.
NYC-WTC_000051318–000051335Folder label: “GCMS X 1/8/02 A 1/10/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Data File : C: \MSDCHEM\1\5973N\02JAN10\00468.D Vial: 5 Acq On 10 Jan 2002 6:07 pm Operator: Sample : 508 scan ext 1/8 Inst : Instrumen Mise : January 10, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 9 Sulfur, mol. (S8) (CAS) $$ ... Concentration Rank 11
R.T. EstConc Area Relative to ISTD R.T.
23.70 0.15 ug/L 79691 Phenanthrene-diO 22.63
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 Sulfur, mol. (S8) (CAS) $$ OCTA-... 256 S8 010544-50-0 40 2 2-Norbornanone, 1- (epithioethyl) . . . 228 C11H1603S 001782-93-0 36 3 PENTAMETHYLENE SULFOXIDE-D4 122 C5H6D4OS 000000-00-0 9 4 5-Nitro-2-furaldoxime $$ 2-Furan... 156 C5H4N2O4 000555-15-7 7 Abundance Scan 1780 (23.696 min): 00468. D (-) m/z 63.95 100.00% 64
160 /Akan 5000 P 96 224 128 , 194 - 1 ' ' I 1 1 1 1 I 1 1 11 1 1 " 1 ' T ' ' ' '
m/z-> 01 44 P ' " I841 " 40 60 80 . Tl 100 120 140 160 180 200 220 240 260 23.40 23.60 23.80 24.00 m/z 159.80 58.40% Abundance #195809: Sulfur, mol. (S8) (CAS) $$ OCTA-SULFUR $$ S8 $$ S... 64 /Aa 5000 192 23.40 23.60 23.80 24.00 128 160 m/z 223.80 33.24% 96
n/z-> Abundance 0 48 1 ' I 1 1 ' 1 1 40 60
64 80 ——— 80 100 120 140 #156398: 2-Norbornanone, 1-(epithioethyl)-7,7-dimethyl-, S... 93 120 160 180 | ■ i ■ • • ■ 224 200 220 । I ■ t ■ ■ ■ ■ ’i ■
240 256 260 "up 23.40 23.60 23.80 24.00 5000 107 m/z 95.90 28.50% 53 164 / 79 151
0+ 34 ■ ■ 1 1 I ■ ■ i 1 " r1 1 TTT ■ ' i ' ' ■ ' i 1 ■ Tl/Z--> 40 60 80 100 120 140 160 180 200 220 240 260 Abundance #17591: PENTAMETHYLENE SULFOXIDE-D4 6|4 23.40 23.60 23.80 24.00 m/ z 64.90 20.90%
5000 120
AAA WwA* Tl/Z-> 0 1 1 I 1 ' 40 Tit 60 l 80 100 103
120 140 160 180 200 220 240 260 23.40 23.60 23.80 24.00 TT
00468.D SCAN508.M Fri Jan 11 10:08:44 2002 Page 11
NYC-WTC_000051332
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NYC-WTC_000051740
GCMS analysis log for sample AE00560 showing surrogate recovery and unknown compounds detected on January 17, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000050774
Laboratory report listing unknown compounds and surrogate recovery for sample AE00106 analyzed on February 7, 2002.
1 shared topics · Same agency, volume and box · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000051586
Laboratory report showing GCMS analysis results for sample AE00613 conducted on February 1, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000050912
Laboratory record documenting GCMS surrogate recovery data for sample AE00281 analyzed on January 10, 2002.
1 shared topics · Same agency, volume and box · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000052291
Laboratory report detailing GCMS scan results for sample AE00844, including detection of unknown compounds and surrogate recovery data.
1 shared topics · Same agency, volume and box · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000052251
Laboratory report showing GCMS analysis of sample AE00842 including surrogate recovery and unknown compounds.
1 shared topics · Same agency, volume and box · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000052311
Laboratory report detailing GCMS scan results for sample AE00841, including detection of unknown compounds and surrogate recovery data.
1 shared topics · Same agency, volume and box · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000050893
Laboratory record documenting GCMS surrogate recovery data for sample AE00280 analyzed on January 10, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000050838
Quality control report for GCMS analysis of sample AE00277 showing surrogate recovery data from January 10, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000051549
Laboratory report showing GCMS analysis results for sample AE00556 conducted on February 1, 2002.
1 shared topics · Same agency, volume and box · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000050754
Laboratory report listing unknown compounds and surrogate recovery for sample AE00108 analyzed on February 7, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000003543
Laboratory report documenting GCMS analysis of sample AE01141 conducted on February 27, 2002.
1 shared non-person entities · 1 shared topics · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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NYC-WTC_000051152
Administrative record from DEP Box 28 documenting GCMS activities at the World Trade Center site in January 2002.
Filed in the same folder
NYC-WTC_000051153
Document header page containing identification codes and metadata for GCMS files processed in early January 2002.
Filed in the same folder
NYC-WTC_000051156
Laboratory report detailing GCMS analysis of sample AE00327 for volatile organic compounds on January 10-11, 2002.
Filed in the same folder
NYC-WTC_000051165
Laboratory report showing GCMS analysis of reference standards used for calibration during January 10-11, 2002 testing.
Filed in the same folder
NYC-WTC_000051179
Laboratory report documenting GCMS blank analysis to verify system cleanliness during January 10-11, 2002 testing.
Filed in the same folder