Laboratory report showing GCMS analysis of sample AE00468 with surrogate recovery data on January 18, 2002.
NYC-WTC_000051318–000051335Folder label: “GCMS X 1/8/02 A 1/10/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Data File : C:\MSDCHEM\1\5973N\02JAN10\00468.D Vial: 5 Acq On : 10 Jan 2002 6:07 pm Operator: Sample : 508 scan ext 1/8 Inst : Instrumen Mise : January 10, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 8 3-Methylchromone $$ 4H-1-Be... Concentration Rank 8
R.T. EstConc Area Relative to ISTD R.T.
23.42 0.18 ug/L 97397 Phenanthrene-dlO 22.63
Hit# of 5 Tentative ID MW MolForm CAS# Qual ---------------- NO 1 3-Methylchromone $$ 4H-1-Benzopy... 160 C10H8O2 000085-90-5 64 AC 2 2,4-Dinitrobenzoic acid $$ Benzo... 212 C7H4N206 000610-30-0 366 3 2-Norbornanone, 1-(epithioethyl)... 228 C11H16O3S 001782-93-0 36 MMTOV 4 Methanesulphonothioic acid 1,5-p... 292 C7H1604S4 000056-00-8 9 Abundance Scan 1756 (23.422 min): 00468.D (-) m/z 63.95 100.00% 64
160 5000 96 224 I ' 1 1 ' I 1 ' 84 128 192 256 23.00 23.20 23.40 23.60 23.80 Of . . । 49 Tn LH - — "TI m/z 159.90 53.89% n/z-> 40 60 80 100 120 140 160 180 200 220 240 260 Abundance #59933: 3-Methylchromone $$ 4H-1-Benzopyran-4-one, 3-methy... 92 1(0 64 131 5000- 77 104 120 23.00 23.20 23.40 23.60 23.80 " z 95.90 24.03%
01 /z-> 40 60 80 100 120 140 160 180 200 220 240 260 Abundance #132098: 2,4-Dinitrobenzoic acid $$ Benzoic acid, 2,4-dinitro 44 UBT 1 1 1 1 ‘"7 I 1 11 ' 1 ' 1 63 75 23.00 23.20 23.40 23.60 23.80 120 168 5000- 92 212 m/z 223.80 19.46%
108
0+ 1.. Ta . 148 ■ । 196 ■ I । 1 ■
./AMA ' ' I ■ ■ i ■ ' "dl n/z-> 40 60 80 100 120 140 160 180 200 220 240 260 Abundance #156398:2-Norbornanone, 1-(epithioethyl)-7,7-dimethyl-, S... 64 93 120 2300 23.20 23.40 23.60 23.80 m/z 161.80 14.67%
5000 107 53 164 79 151
/z-> 0 34 ■ 1 1 1 40 ' 1 I 60 80 100 120 140 160 180 200 220 240 260 . ....... „A.A/. 23.00 23.20 23.40 23.60 23.80
00468.D SCAN508.M Fri Jan 11 10:08:43 2002 Page 10
NYC-WTC_000051331
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NYC-WTC_000051740
GCMS analysis log for sample AE00560 showing surrogate recovery and unknown compounds detected on January 17, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000050774
Laboratory report listing unknown compounds and surrogate recovery for sample AE00106 analyzed on February 7, 2002.
1 shared topics · Same agency, volume and box · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000051586
Laboratory report showing GCMS analysis results for sample AE00613 conducted on February 1, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000050912
Laboratory record documenting GCMS surrogate recovery data for sample AE00281 analyzed on January 10, 2002.
1 shared topics · Same agency, volume and box · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000052291
Laboratory report detailing GCMS scan results for sample AE00844, including detection of unknown compounds and surrogate recovery data.
1 shared topics · Same agency, volume and box · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000052251
Laboratory report showing GCMS analysis of sample AE00842 including surrogate recovery and unknown compounds.
1 shared topics · Same agency, volume and box · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000052311
Laboratory report detailing GCMS scan results for sample AE00841, including detection of unknown compounds and surrogate recovery data.
1 shared topics · Same agency, volume and box · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000050893
Laboratory record documenting GCMS surrogate recovery data for sample AE00280 analyzed on January 10, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000050838
Quality control report for GCMS analysis of sample AE00277 showing surrogate recovery data from January 10, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000051549
Laboratory report showing GCMS analysis results for sample AE00556 conducted on February 1, 2002.
1 shared topics · Same agency, volume and box · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000050754
Laboratory report listing unknown compounds and surrogate recovery for sample AE00108 analyzed on February 7, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000003543
Laboratory report documenting GCMS analysis of sample AE01141 conducted on February 27, 2002.
1 shared non-person entities · 1 shared topics · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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NYC-WTC_000051152
Administrative record from DEP Box 28 documenting GCMS activities at the World Trade Center site in January 2002.
Filed in the same folder
NYC-WTC_000051153
Document header page containing identification codes and metadata for GCMS files processed in early January 2002.
Filed in the same folder
NYC-WTC_000051156
Laboratory report detailing GCMS analysis of sample AE00327 for volatile organic compounds on January 10-11, 2002.
Filed in the same folder
NYC-WTC_000051165
Laboratory report showing GCMS analysis of reference standards used for calibration during January 10-11, 2002 testing.
Filed in the same folder
NYC-WTC_000051179
Laboratory report documenting GCMS blank analysis to verify system cleanliness during January 10-11, 2002 testing.
Filed in the same folder