GCMS analysis results for sample AE00840, Feb 4 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

■ Data File : C: \MSDCHEM\1\5973N\02JAN31\00840.D Vial: 4 Acq On : 31 Jan 2002 , 5:11 pm Operator: Sample : 508 scan Inst : Instrumen Mise : January 31, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\l-..\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 13 Cyclic octaatomic sulfur Concentration Rank 12

R.T. EstConc Area Relative to ISTD R.T.

26.00 0.05 ug/L 40579 Phenanthrene-dl0 22.65

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Cyclic octaatomic sulfur 256 S8 010544-50-0 91 2 Sulfur, mol. (S8) (CAS) $$ OCTA-... 256 S8 010544-50-0 91 3 Sulfur, mol. (S8) (CAS) $$ OCTA-... 256 S8 010544-50-0 91 4 Sulfur, mol. (S8) (CAS) $$ OCTA-... 256 S8 010544-50-0 90 Abundance Scan 1982 (26.002 min): 00840.D (-) m/z 64.00 100.00% 64

5000 128 160 256 96 192 25.60 25.80 26.00 26.20 26.40 44 1......... ot ■ ■ > I I ■ '| I....... 1, , , . 1..... m/z 127.90 40.91% m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 Abundance #195804: Cyclic octaatomic sulfur 64

5000 TTnuT > ' i ' I"' ' । ■ । 25.60 25.80 26.00 26.20 26.40 m/z 159.90 23.59% 128 160 192 256

/z-> 0t 34 40 i 1 1 ' 1 1 60 80 100 120 140 160 180 200 220 240 0...... ।.......?1260 Abundance #195807: Sulfur, mol. (S8) (CAS) $$ OCTA-SULFUR $$ S8 $$ S... 64 25.60 25.80 26.00 26.20 26.40 5000 m/z 255.80 23.27% 128 256 96 160 192 34 48 0 • ' i ’ ' ■ ' i ■ ■ ■ i ■ ’ i Tu m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 Abundance #195802: Sulfur, mol. (S8) (CAS) $$ OCTA-SULFUR $$ S8 $$ S... 64 25.60 25.80 26.00 26.20 26.40 m/z 191.80 17.48%

5000

128 160 256

m/z—> 0 34 ■ ■ i ■ 1 1 ' i 40 60 L79— 80 100 - — 120 192

140 160 180 200 224 1 1 1 1 ' ' ' 1 1 1 1 1 1 1 1 220 240 1, 260 T 25.60 25.80 26.00 26.20 26.40 T

30840.D SCAN508.M Fri Feb 01 09:19:22 2002 Page 15

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