GCMS analysis results, Sample AE02085, Mar 2002

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Laboratory report for GC/MS analysis of sample AE02085 conducted on March 25, 2002.

NYC-WTC_000012226–000012234

Folder label: “GCMS X 3-1-02 A 3-20-02 MANY RERNNS”

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NYC 9/11 Public Portal Document Library Search Compound Report

. Data File : C:\MSDCHEM\l\DATA\031902\2085.D Vial: 21 Acq On : 20 Mar 2002 5:39 am Operator: McLean Sample : RE-INJ 3/1 Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\1\5973N\5080302.M (RTE Integrator) Title : Quantitation For Method 508gcscan Library : C:\DATABASE\WILEY7N.L

Peak Number 1 Sulfur, mol. (S8) (CAS) $$ ... Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

26.01 0.42 ug/L 184732 Phenanthrene-dlO 22.50

Hit# of 5 Tentative ID MW MolForm CAS# Qual 6— * 1 Sulfur, mol. (S8) (CAS) $$ OCTA-... 256 S8 010544-50-0 94 2 Cyclic octaatomic sulfur 256 S8 010544-50-0 91, 3 Sulfur, mol. (S8) (CAS) $$ OCTA-... 256 S8 010544-50-0 91 4 Sulfur, mol. (S8) (CAS) $$ OCTA-... 256 S8 010544-50-091 Abundance Scan 2528 (26.006 mln): 2085.D (-) m/z 63.95 100.00% 64

5000

96 128 160 256 111 KTrp TTi । 1111 192 25.60 25.80 26.00 26.20 26.40 I 1 224 | m/z 127.90 24.20% 0 ‘1444414/144/ " I ’' 1**’’$* ‘ ‘ l “ ■''' 1 ‘1 ‘ “ i1 ■ ■' i “ rp-r m/z--> 20 40 60 80 100 120 140 160 180 200 220 240 260 Abundance #195803: Sulfur, mol. (S8) (CAS) $$ OCTA-SULFUR $$ S8 $$ S... 64

5000 28 i ■ ■ ■ ■ i ‘ ‘ ■ ■ i ■ •

256 25.60 25.80 26.00 26.20 26.40 160 m/z 255.80 23.89% 128 192 96

rn/z-> 01‘IT :20 44—7 40 601 | ■ **I‘ I“>•i• ■ ‘ i 80 100 120 140 160 180 200 220 240 260 —24 TT • ■ i • • r' i" ■ ■ i1 ■ ■ ■ i “

Abundance #195804: Cyclic octaatomic sulfur 61

25.60 25.80 26.00 26.20 26.40 5000 m/z 159.80 21.99%

32 96 «8 160 192 256 0 i■•■■i■ 1 78 | 110 |, .». 11.»I p . J i I, k I»I. J'i i j, I 224 .. ।. r. ।.... 11....... I |.. m/z—> 20 40 60 80 100 120 140 160 180 200 220 240 260 Abundance #195802: Sulfur, mol. (S8) (CAS) $$ OCTA-SULFUR $$ S8 $$ S... 64 25.60 25.80 26.00 26.20 26.40 m/z 95.90 19.82%

5000

32 96 128 160 192 256 , ,|. 461 1 . 78 I. 110 |, 224 01 1 ■ । !'■ | । ■ ।• • । ri 11... i j, ■ ■. ।. i >, ।, 11000—0090 TP /z—> 120 40 60 80 100 120 140 160 180 200 220 240 260 25.60 25.80 26.00 26.20 26.40

2085.D 5080302.M Thu Mar 21 08:20:33 2002 Page 3

NYC-WTC_000012233

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