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Document / 16 pages

GCMS blank analysis results for sample AD31647, Jan 2002

Machine-extracted title · confidence 100%

Blank analysis report for GCMS testing of sample AD31647 confirming no contamination above detection limits.

NYC-WTC_000050189–000050204

Folder label: “GCMS X 1/3/02 A 1/22 - 1/23/02

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\MSDCHEM\1\5973N\02JAN22\0103BA.D Vial: 1 Acq On : 22 Jan 2002 10:32 am Operator: Sample : lab blank 1/3 a Inst : Instrumen Mise : January 22, 2002 Multipir: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 11 Sulfur, mol. (S8) (CAS) $$ ... Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T.

26.01 3.04 ug/L 1767780 Phenanthrene-dl0 22.63

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Sulfur, mol. (S8) (CAS) $$ OCTA-... 256 S8 010544-50-0 96 2 Cyclic octaatomic sulfur $$ Sulf... 256 S8 010544-50-0 95 3 Sulfur, mol. (S8) (CAS) $$ OCTA-... 256 S8 010544-50-0 94 4 Cyclic octaatomic sulfur 256 S8 010544-50-0 91 Abundance Scan 1983 (26.014 min): 0103BA.D (-) m/z 64.00 100.00% 64

128 5000 160 256 ......... .. .......... 96 192 25.60 25.80 26.00 26.20 26.40 iz-> 36 I 76 _ 1 1 i • ' • • i • ‘ 1 i ■ 1 40 60 80 100 —P i 224 ' tanakIati TT 120 140 160 180 200 220 240 260 m/z 127.90 56.16% Abundance #195807: Sulfur, mol. (S8) (CAS) $$ OCTA-SULFUR $$S8$$ S... 64

5000 128 256 25.60 25.'80 26.00 26.20 26.40 96 160 m/z 255.80 48.03% 192

niz-> 34 48 ■ ■ i 1 1 ■ ■ i 40 60 1 ■ ■ i ■ ■ 80 i ■ ■ ■ ‘ i 1 i 100 120 140 160 180 200 220 240 224 ■ 1 ■ * ■ * । ■ * i ■ l ■ t I 260 Abundance #195805: Cyclic octaatomic sulfur $$ Sulfur, mol. (S8) $$ ... 64 ____________ / ___________ 256 i ■ ‘ ■ i ■ ■ • ' i • ■ 1 1 I ' ' 1 ' i 1 ' 25.60 25.80 26.00 26.20 26.40 128 160 5000 192 m/z 159.90 45.41%

96 224 34 | I.. I I.... , iz-> ■ ' I 1 1 ■ ' i -r-r-r-p-r 40 60 80 i ■1 ■11' 1 1 i ' 1 100 120 140 160 180 200 220 240 T- i i i < । i i ' i 1 1 ' 1 i 1 T-r-p-r TT 260 Abundance #195806: Sulfur, mol. (S8) (CAS) $$ OCTA-SULFUR $$ S8 $$ S... nnn—nm—nmnBB—nn/B—Bon 64 256 25.60 25.80 26.00 26.20 26.40 m/z 191.80 26.90% 160 128 5000

96 192 224 34 - ------- ■ 00 i • • ■ ■ i ■ ‘ i • • i • • ■ 11 1 iz—> 40 60 80 100 120 140 160 180 200 220 240 260 25.60 25.80 26.00 26.20 26.40

0103BA.D SCAN508.M Thu Jan 24 13:46:54 2002 Page 13

NYC-WTC_000050203

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NYC-WTC_000050203Source: NYC Law Department, mirrored locally

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machine-extracted · confidence unavailable · Check page ↗
DEP GCMS data table, Jan-Feb 2002 · Box DEP Box 12

NYC-WTC_000004494

Multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.

2 shared non-person entities · 1 shared topics · similarity 0.994

machine-extracted · confidence unavailable · Check page ↗
DEP GCMS data table, Jan-Feb 2002 · Box DEP Box 12

NYC-WTC_000004935

Multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.

2 shared non-person entities · 1 shared topics · similarity 0.994

machine-extracted · confidence unavailable · Check page ↗

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