GC/MS analysis report, sample AE03178, March 2002

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Gas chromatography-mass spectrometry analysis results for sample AE03178, completed March 22, 2002 by analyst DLV.

NYC-WTC_000011135–000011143

Folder label: “GCMS X 2/12/02 A 3/19/02”

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NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C:\MSDCHEM\1\DATA\031802\3178.D Vial: 10 Acq On : 19 Mar 2002 9:33 am Operator: McLean Sample : GC/MS SCAN 3/6 FB Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\1\5973N\5080302.M (RTE Integrator) Title : Quantitation For Method 508gcscan Library : C: \DATABASE\WILEY7N. L

Peak Number 1 Sulfur, mol. (S8) (CAS) $$ ... Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

26.01 0.40 ug/L 155094 Phenanthrene-dlO 22.50

Hit# of 5 Tentative ID MW Mol Form CAS# Qual l Sulfur, mol. (S8) (CAS) $$ OCTA-... 256 S8 010544-50-0 95 2 Sulfur, mol. (S8) (CAS) $$ OCTA-... 256 S8 010544-50-0 91 3 Sulfur, mol. (S8) (CAS) $$ OCTA-... 256 S8 010544-50-0 91 4 Cyclic octaatomic sulfur 256 S8 010544-50-0 91 Abundance Scan 2528 (26.005 min): 3178.D (-) m/z 64.00 100.00% 64

5000

128 96 160 192 256 25.60 25.80 26.00 26.20 26.40 Ol i “ • ■ i " ' • i • i ■ ■ n11' i' 1___ m-j-rr j • • i • ■ T11 1 1 111 1 1 11 1 r TTT ,.....224.... m/z 127.90 26.52% miz—> :20 40 60 80 100 120 140 160 180 200 220 240 260 Abundance #195803: Sulfur, mol. (S8) (CAS) $$ OCTA-SULFUR SS S8 $$ S... 64

5000 28 256 25.60 25.80 26.00 26.20 26.40 160 m/z 159.80 21.55% 96 128 192 44 ........ |l.,,,|.,|i.. 224, ... 0 I’ TIP m/z—> 20 40 60 80 100 120 140 160 180 200 226' '246' 260 Abundance #195807: Sulfur, mol. (S8) (CAS) $$ OCTA-SULFUR $$ S8 $$ S... 64 TCIIunnr PAyonagan 25.60 25.80 26.00 26.20 26.40 5000 m/z 96.00 19.06% 128 256 96 160 192 34 48 0 i • ■ • ■ i ■1 ■ ■ i | 80 , i *■ ■ •। ■ H 1........... 1,.......... 224 ।ri 1111111111111 iz—> 20 40 60 80 100 120 140 160 180 200 220 240 260 Abundance #195802: Sulfur, mol. (S8) (CAS) $$ OCTA-SULFUR $$ S8 $$ S... 64 25.60 25.80 26*00 26.20 26.40 m/z 255.80 18.76%

5000

32 g 96 110 128 160 192 256 . 46 224 — 0 m 1,1111'l 110 । > > । > ■ ■ 1111 l’i 111111 I I 11 111 F| > I T8T Tl/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 25.60 25.80 26.00 26.20 26.40

5178.D 5080302.M Tue Mar 19 21:35:34 2002 Page 3

NYC-WTC_000011142

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