GCMS analysis results for sample AE01047, March 2002

NYC 9/11 Public Portal Document

Data File : C:\MSDCHEM\l\DATA\022802\01047FB.D Vial: 16 Acq On : 28 Feb 2002 11:15 pm Operator: McLean Sample : GC MS SCAN 2/27 Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\1\5973N\5080202.M (RTE Integrator) Title : Quantitation For Method 508gcscan Library : C:\DATABASE\WILEY7N.L

Peak Number 2 .beta.-iso-methyl ionone Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T. j 35.68 1.22 ug/L 298183 Perylene-dl2 34.20

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 .beta.-iso-methyl ionone 206 C13H18O2 000000-00-0 49 2 Anthracene, 9-dodecyltetradecahy... 360 C26H48 055401-75-7 47 3 .beta. N METHYL IONONE 206 C14H22O 000127-43-5 46 4 2-((E,E-2,4-Hexadienoyl))-cycloh... 192 C12H16O2 _______ 088924-70-3 42 Abundance Scan 3595 (35.683 min): 01047FB.D (-) m/z 191.20 “100.00% 191

95 5000 55 123

35.40 35.60 35.80 36.00 0 . , ual , 218 i ■ ’■ ■ 398 ,1,1 m/z 95.10 51.16%

U m/z~> 50 100 150 200 250 300 350 400 Abundance #124104: .beta.-iso-methyl ionone 191 AAvWW

5000 ■ ‘ ■ i 1 ' ■ 1 t 1 ' 1 1 i ‘ ■ i ■ ■ ■ ■ 35.40 35.60 35.80 36.00 43 135 163 m/z 81.10 48.69% 69 95

01 K 4 i- 44 1-4 m/z->__ 50 100 150 200 250 300 350 400 Abundance #306717: Anthracene, §-dodecyltetradecahydro- SS 9-n-Dodec... 191 WWWA 95 35.40 35.60 35.80 36.00 m/z 55.10 40.31%

_N 5000 43 i 67

135

01 ,.1/44*2+4,441634 , 212 236 264 303 330 360 m/z-> 50 100 150 200 250 300 350 400 Abundance #124644: .beta. N METHYL IONONE 191 T T T 35.40 35.60 35.80 36.00 m/z 177.20 39.26%

5000

57

0 91 121 149

dd .bl + 14 « A, : 1 wwA m/z-> 50 100 150 200 250 300 350 400 35.40 35.60 35.80 36.00

1047FB.D 5080202.M Wed Mar 13 11:03:33 2002 Page 4

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