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GCMS analysis results for sample AE03472, March 2002

Machine-extracted title · confidence 95%

Laboratory report documenting GCMS analysis of sample AE03472 for unknown compounds and surrogates on March 14, 2002.

NYC-WTC_000038473–000038483

Folder label: “GCMS X 2/26/02 A 2/28/02

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NYC 9/11 Public Portal Document

Data File C:\MSDCHEM\l\DATA\022802\03472.D Vial: 21 . Aeq On 1 Mar 2002 4:58 am Operator: McLean * Sample Inst : Instrumen Mise : Multiplr: 1-00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\1\5973N\5080202.M (RTE Integrator) Title : Quantitation For Method 508gcscan Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 2 Acetic acid, (2,4,5-trichlo... Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

33.40 0.99 ug/L 247397 Perylene-dl2 34.20

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Acetic acid, (2,4,5-trichlorophe... 366 C16H21C13O3 025168-15-4 22 2 trans-1-Butyl-2-methylcyclopropane 112 C8H16 038851-70-6 22 3 Isooctane, (ethenyloxy)- 156 C10H20O 037769-62-3 22 4 4-Undecanol, 7-ethyl-2-methyl- (... 214 C14H30O 000103-20-8 14 Abundance Scan 3343 (33.398 min): 03472.D (-) m/z 185.10 100.00% 57 185

5000 112 83 i • ■ ■ ■ i * ■ • • i • ■ 33.00 33.20 33.40 33.60 33.80

m/z—> 0- 9 50 ALL 100 139

150 । IT 200 250 300 297 i

350 m/z 57.10 97.10%

Abundance #310394: Acetic acid, (2,4,5-trichlorophenoxy)-, isooctyl... 57

87 5000 33'00 33.20 33.40 33.60 33.80 m/z 55.10 53.60%

■n/z-> 0 all 50 100 111 150 143 । I81 2112311 2i6 200 250 300 292 326 368, 350 Abundance #14056: trans-1-Butyl-2-methylcyclopropane 55 i ‘ ■ 1 11 ■ 33.00 33.20 33.40 33.60 33.80 5000 m/z 71.10 44.61% 83 112

— i 0- TIt •n/z-> 50 100 150 200 250 300 350 Abundance #55956: Isooctane, (ethenyloxy)- 57 33.00 33'20 33.40 33.60 33.80 m/z 70.10 43.02%

5000

29 84 110

0 ■ —H 1lI' i ‘ i» < l • 1 । ' i ■ • ■ ■ j • • m/z—> 50 100 150 200 250 300 350 33.00 33.20 33.40 33.60 33.80

03472.D 5080202.M Wed Mar 13 06:56:00 2002 Page 4

NYC-WTC_000038482

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NYC-WTC_000038482Source: NYC Law Department, mirrored locally

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