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GCMS analysis results for sample AE03472, March 2002

Machine-extracted title · confidence 95%

Laboratory report documenting GCMS analysis of sample AE03472 for unknown compounds and surrogates on March 14, 2002.

NYC-WTC_000038473–000038483

Folder label: “GCMS X 2/26/02 A 2/28/02

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NYC 9/11 Public Portal Document WBsp/** **** AWUEW*s

Data File C:\MSDCHEM\1\DATA\022 8 02\03472.D Vial: 21 , Aeq On 1 Mar 2002 4:58 am Operator: McLean Sample Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\1\5973N\5080202.M (RTE Integrator) Title : Quantitation For Method 508gcscan Library : C:\DATABASE\WILEY7N.L

Peak Number 1 Cyclopentasiloxane, decamet... Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

12.08 1.35 ug/L 446412 Naphthalene-d8 13.05

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 86 2 Cyclopentasiloxane, decamethyl- 370 C10H3005S15 000541-02-6 74 •3 Phenethylamine, N-methyl-.beta.,... 399 C18H37NO3Si3 010538-85-9 47 4 3,4-DIHYDROXYMANDELIC ACID-TETRATMS 472 C20H40O5S14 000000-00-0 38 Abundance Scan 993 (12.083 mln): 03472.D (-) m/z 73.10 100.00% 73

5000 267 355 1111111TI । 'i ■ 111 > 11 45 11.80 12.00 12.20 12.40 0- — 133154 , +123223, + , 323 m/z 267.00 48.69% m/z-> 50 100 ' ’ 150 ' 200 250' — 1 300 11 350 Abundance #313068: Cyclopentasiloxane, decamethyl- 73

355 267 5000 11.80 12.00 12.20 12.40 m/z 355.10 38.71% 45 207 . I 323 , - 0- t । . . . । TPT 1 # t "i r * r * * — T * rr + । miz-> 50 100 150 200 250 300 350 Abundance #313065: Cyclopentasiloxane, decamethyl- 73 —. 1. ।.... । ।11 111 111 11.80 12.00 12.20 12.40 5000 m/z 356.10 15.36% 267 355 45 0- 96 133 165 123 223 247,1 293 323 +4 I TT ' ’ m/z-> 50 100 150 200 250 300 350 Abundance #331718: Phenethylamine, N-methyl-beta.,3,4-tris(trimethy... 73 11.80 12.00 12.20 12.40 m/z 268.00 11.30%

5000 355

44

0 —*4 ।« 4 93 116 147 193 220 267 294 1 TT# 1 1 ’ TT ITT r j —IT TT — r 384 m/z—> 50 100 150 200 250 300 350 11.8012.00 12.20 12.40

33472.D 5080202.M Wed Mar 13 06:55:59 2002 Page 3

NYC-WTC_000038481

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NYC-WTC_000038481Source: NYC Law Department, mirrored locally

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