GCMS quantitation results for sample AE03439, March 2002

NYC 9/11 Public Portal Document

Data File C:\MSDCHEM\l\DATA\022802\03439.D Vial: 26 Acq On 1 Mar 2002 9:04 am Operator: McLean • Sample Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\1\5973N\5080202.M (RTE Integrator) Title : Quantitation For Method 508gcscan Library : C:\DATABASE\WILEY7N.L

Peak Number 1 Cyclopentasiloxane, decamet... Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

12.08 2.35 ug/L 604011 Naphthalene-d8 13.05

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 64 2 Phenethylamine, N-methyl- .beta.____ 399 C18H37NO3S13 010538-85-9 47 3 3,4-DIHYDROXYMANDELIC ACID-TETRATMS 472 C20H4005Si4 . 000000-00-0 38 4 N-(Trifluoroacetyl)-N,O,O',O' 1-t... 553 C22H42F3NO4Si4 000000-00-038 Abundance Scan 993 (12.083 mln): 03439.D (-) m/z 73.10 100.00% 75

5000 267 355

■' I ■ ■ ■' l —...... 45 11.8012.00 12.20 12.40 - 108 154 193 223 4 323 m/z 267.00 50.07% 0- 1I1*fr ' 1 I TIT > I ‘ • i ■ ■ ■ 1 i ■ ■ m/z-> 50 100 150 200 250 300 350 400 450 Abundance #313068: Cyclopentasiloxane, decamethyl- 73

355 267 5000 T—mT 11.80 12.00 12.20 12.40 m/z 355.10 41.01% 45 207 , 323 0-— + m/z—> 50 100 150 200 250 300 350 400 ' ' 450 Abundance #331718: Phenethylamine, N-methyl-beta.,3,4-tris(trimethy... 73

11.80 12.00 12.20 12.40 5000 m/z 356.10 14.12% 355

44 J , । 116 147 193220 267 294 384..... 01 I * • t T • ’» IT i । TIIT r i *i TT r il । * miz-> Abundance 50 100 150 200 250 300 350 1400 450 #361636: 3,4-DIHYDROXYMANDELIC ACID-TETRATMS 0 ’111111111 73 11.8012.00 12.20 12.40 m/z 268.00 11.12% 355 5000

45 147 | 193 267 295 429 457 0T 1 i + r rT —f —1 IBr IT 1 .. I ' I''' ■ I ■ ■ m/z—> 50 100 150 200 250 300 350 400 450 11.80 12.00 12.20 12.40

3439.D 5080202.M Wed Mar 13 06:50:10 2002 Page 3

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