NYC-WTC_000052620
Laboratory report documenting GCMS analysis of sample AE01045 conducted on March 14, 2002.
1 shared topics · Same agency, volume and box · similarity 0.992
machine-extracted · confidence unavailable · Check page ↗Document / 13 pages
GCMS analysis results for sample AE01047, March 2002
Machine-extracted title · confidence 100%Laboratory report documenting GCMS analysis of sample AE01047 conducted on March 14, 2002.
NYC-WTC_000052653–000052665Folder label: “GCMS X 1/15/02 A 2/28/02”
Page image
OCR text
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Data File : C:\MSDCHEM\l\DATA\022802\01047FB.D Vial: 16 Acq On : 28 Feb 2002 11:15 pm Operator: McLean Sample : GC MS SCAN 2/27 Inst Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P
Quant Method : C:\MSDCHEM\1\5973N\5080202.M (RTE Integrator) Title : Quantitation For Method 508gcscan Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 3 .beta.-iso-methyl ionone Concentration Rank 1
R.T. EstConc Area Relative to ISTD R.T.
36.43 1.93 ug/L 471699 Perylene-d12 34.20
Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 .beta.-iso-methyl ionone 206 C13H1802 000000-00-0 70 2 .beta.-methyl ionone 206 C14H22O 000000-00-0 60 3 2,4,5,5,8a-Pentamethyl-6,7,8,8a-... 206 C14H220 000000-00-0 52 4 3,6-Dimethyl-2- (1-(trimethylsily . . . 206 CllH18N2Si 000000-00-0 50 Abundance Scan 3677 (36.427 min): 01047FB.D (-) m/z 191.15 100.00% 191
5000 95 55 123
andis 36.20 36.40 36.60 36.80
J j , 231 259281 412 m/z 95.10 45.66% । i 0 i "I |“i l r i । I । । > | m/z-> 50 100 150 200___ 250 ..... 300 350 400 Abundance #124104: .beta.-iso-methyl ionone 191
mMMM WA 5000 T 36.20 36.40 36.60 36.80
J 43 135 163 m/z 81.10 42.49% 95 69 0 1 J l It m/z-> 50 100 150 200___ 250...._300___ 350___ 400 Abundance #124627: .beta.-methyl ionone 191
—> > - > ।111111 ’ ’111 ’' TTT’’ 36.20 36.40 36.60 36.80 m/z 55.10 32.30% 5000 57
107 149 29 : , 81 , I 01 1 1 ’ i 44444.1 2, ), m/z-> 50 100 150 200 250 300 350 400 * Abundance #124787: 2,4,5,5,8a-Pentamethyl-6,7,8,8a-tetrahydro-5H-chr... 191 ' ' ' ' I ' ' ' ' I ' ' ' ' I ' ' ' ' I ' ' b 36.20 36.40 36.60 36.80 m/z 69.10 31.72%
5000
m/z-> 0 43 I 69 91 , J 4,4 4 1 " | " " 1 bl >ll 50 100 123 149
150 200 250 300 350 400 M T Tr 36.20 36.40 36.60 36.80
01047FB.D 5080202.M Wed Mar 13 11:03:34 2002 Page 5
NYC-WTC_000052662
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NYC-WTC_000052662Source: NYC Law Department, mirrored locally
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