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GCMS analysis results for sample AE00466, Jan 18 2002

Machine-extracted title · confidence 100%

Laboratory report documenting gas chromatography-mass spectrometry analysis of environmental sample AE00466 conducted on January 18, 2002.

NYC-WTC_000051263–000051282

Folder label: “GCMS X 1/8/02 A 1/10/02

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Scanned page image, NYC-WTC_000051280
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NYC 9/11 Public Portal Document

Library Search Compound Report

. Data File : C:\MSDCHEM\1\5973N\02JAN10\00473.D vial: 8 Acq On 10 Jan 2002 8:36 pm Operator: Sample : 508 scan ext 1/8 Inst : Instrumen Mise : January 10, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\l-..\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 12 13(16),14-LABDIEN-8-OL Concentration Rank 10

R.T. EstConc Area Relative to ISTD R.T.

35.80 0.43 ug/L 225447 Perylene-dl2 34.42

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 13(16),14-LABDIEN-8-OL 290 C2OH340 000000-00-0 47 NO 2 2,4,5,5,8a-Pentamethyl-6,7,8,8a-... 206 C14H220 000000-00-0 43 (T 3 .beta.-iso-methyl ionone 206 C13H1802 000000-00-0 43 ( 4 .beta. N METHYL IONONE 206 C14H220 000127-43-5 43 y Abundance Scan 2840 (35.798 min): 00473. D (-) m/z 191.20 100.00% 191

5000 81 109 , 136 163 35'40 35.60 35.80 36.00 36'20 -A ALL

A 41 I 365383 0- Tr t 209227245263, 291...... 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 400 H m/z 177.20 40.41% n/z-> Abundance #238717:13(16),14-LABDIEN-8-OL 191 69

95 5000 123 35.40 35.60 35.80 36.00 36.20 m/ z 81.10 38.48% 149

m/z—> 0- ।"111 IL Xu. 272 ■ i"■ ■ i।■1 ■ i• ■ I■ i।"i"‘ ■ i""i""i■' 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 400 Abundance #124787: 2,4,5,5,8a-Pentamethyl-6,7,8,8a-tetrahydro-5H-chr... 191

35.40 35.60 35.80 36.00 36.20 5000 m/z 95.10 36.17%

123 149 0 .........9.1 ’1I,’t r ■" r ■" r1111" " i"111 n/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 400 Abundance #124104: beta.-iso-methyl ionone 191 35.40 35.60 35.80 36.00 36.20 m/ z 69.10 23.52%

5000

135 163 69 95 m/z-> 0 " r' " I " " i ■11' i " —HH++ .7/011000210 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 400 35.40 35'60 35.80 36.00 '36.20

00473.D SCAN508.M Fri Jan 11 10:09:10 2002 Page 14

NYC-WTC_000051280

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NYC-WTC_000051280Source: NYC Law Department, mirrored locally

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