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GCMS analysis results for sample AE00466, Jan 18 2002

Machine-extracted title · confidence 100%

Laboratory report documenting gas chromatography-mass spectrometry analysis of environmental sample AE00466 conducted on January 18, 2002.

NYC-WTC_000051263–000051282

Folder label: “GCMS X 1/8/02 A 1/10/02

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Scanned page image, NYC-WTC_000051279
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OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Library Search Compound Report

. Data File : C:\MSDCHEM\1\5973N\02JAN10\00473.D Vial: 8 Acq On : 10 Jan 2002 8:36 pm Operator: Sample : 508 scan ext 1/8 Inst : Instrumen Mise : January 10, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N. L ********************************************************************* Peak Number 11 Eicosane (CAS) $$ n-Eicosane Concentration Rank 7

R.T. EstConc Area Relative to ISTD R.T.

27.84 1.35 ug/L 894033 Chrysene-dl2 30.50

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Eicosane (CAS) $$ n-Eicosane 282 C20H42 000112-95-8 94 2 Tetradecane (CAS) $$ n-Tetradeca... 198 C14H30 000629-59-4 93 3 Docosane 310 C22H46 000629-97-0 91 4 Heneicosane (CAS) $$ n-Heneicosane 296 C21H44 000629-94-7 91 Abundance Scan 2143 (27.840 min): 00473.D (-) m/z 57.10 100.00% 57 71

85 5000 43

99 113127 27.60 27.80 28.00 28.20 - — I rl .1 J m-r tm-ti 141155169183197 1 215 231245 262276 1 1111 *1 .., . ... rri 293 317 FITT T TTTTT m/z 71.10 76.69% 0 m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 Abundance #228986: Eicosane (CAS) $$ n-Eicosane 57 71

5000 85 27.60 27.80 28.00 28.20 QQ m/z 85.1.0 50.73% । 113127141155169183197 254 282 0 । I nI il J I i । । .i -0 | TIr m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 Abundance #113298: Tetradecane (CAS) $$ n-Tetradecane $$ Isotetradecane 43 57 27'60 27.80 28.00 28'20" 71 m/ z 43.10 39.25% 5000 85

99 113127_____100 1# 199 198 i. 0- 1’1 1 ■।111'i'11■।'■111111' 11 ■ ■ ■ । ■' ■ 'i ■ ■ ■ ■ i ■'' ■ i' ‘' ■ । i ' ■ ' ■ i ' ‘ ' i ' ' m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 Abundance #261313: Docosane ---- dnTTTTETTTTTET 57 27.60 27.80 28.00 28.20 71 m/z 99.10 19.26% 5000 85 _AM/WA 99

0 PPT T’T Il 13127141155169183 210 T’090rmn’f0—’1’01’n01’—’’0’n’l’"’0—ITrr 254 310 m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 27.60 27.80 28.00 28.20

00473.D SCAN508.M Fri Jan 11 10:09:10 2002 Page 13

NYC-WTC_000051279

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NYC-WTC_000051279Source: NYC Law Department, mirrored locally

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