GCMS analysis results for sample AD31639, Jan 28 2002

NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\MSDCHEM\1\5973N\02JAN17\31639.D Vial: 2 Acq On : 17 Jan 2002 3:39 pm Operator: Sample : 508 scan Inst : Instrumen Mise : January 17, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1. . .\SCAN5 08. M (RTE Integrator) Title : 508 scan method -7 7? Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 7 Heneicosane $$ n-Heneicosane Concentration Rank 4 R.T. EstConc Area Relative to ISTD R.T. 33.26 0.85 ug/L 390682 Perylene-d12 34.42 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Heneicosane $$ n-Heneicosane 296 C21H44 000629-94-7 91 2 Eicosane 282 C20H42 000112-95-8 90 3 Pentacosane 352 C25H52 000629-99-2 90 4 Nonacosane 408 C29H60 000630-03-5 90 Abundance Scan 2618 (33.263 min): 31639.D (-) m/z 57.10 100.00% 57 71 43 85 5000

1. 0 M . 99 119 33.00 33.20 33.40 33.60 niz-> oM a.A1 127 141 155 169... 207 .......... 276 I . ’ * 1* . I •,/41***117***14**’1**’*I+’**I***’1*’*’I+ — 40 60 80 100 120 140 160 180 200 220 240 260 280 300 m/z 71.10 66.01% Abundance #245745: Heneicosane $$ n-Heneicosane 57 71 85 5000 33.00 33.20 33.40 33.60 99 m/z 43.10 52.50% 0-1’......... 1’4461* ■ || 11 113127 141 155 ‘I 1 ■1' i 288 296 ' i ■ ■ ■ ■ i ■ ■ ■ ■ i ■ ■1111'' ■ i ■ ■ ■ ■ i ■ ■ ■ ■ i • ■ ■ ■ i ■''11 ■ niz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #228992: Eicosane 43 57 MA 71 ‘' 33.00 33.20 33.40 33.60 1 5000 m/z 85.10 51.81% 85

miz-> 0- IIT 40 — 60 80 1 100.................................. .,7 120 140 160 180 200 220 240 260 280 300 Abundance #300499: Pentacosane I W 43 57 33.00 33.20 33.40 33.60 m/z 55.10 23.48%

V 71 5000 85

nz—> OP 11 20 113127 141 155 169 183 197 211 . .................. AAAAMA.MMM 40 60 80 100 120 140 160 180 200 220 240 260 280 300 33.00 33.20 33.40 33.60

31639.D SCAN508.M Tue Jan 22 08:37:09 2002 Page 9

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