GCMS analysis results for sample AE00614, Feb 2002

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Library Search Compound Report

. Data File : C:\MSDCHEM\1\5973N\02JAN29\00614.D Vial: 3 Acq On : 29 Jan 2002 4:17 pm Operator: Sample : 508 scan Inst : Instrumen Mise : January 29, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 12 Octadecane, 3-ethyl-5-(2-et... Concentration Rank 8 R.T. EstConc Area Relative to ISTD R.T.

35.74 0.13 ug/L 93410 Perylene-dl2 34.42 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Octadecane, 3-ethyl-5-(2-ethylbu... 366 C26H54 055282-12-7 72 2 Dotriacontane 451 C32H66 000544-85-4 64 3 Octadecane 254 C18H38 000593-45-3 59 4 Heneicosane (CAS) $$ n-Heneicosane 296 C21H44 000629-94-7 59 Abundance Scan 2835 (35.740 min): 00614.D (-) m/z 57.10 100.00%

L 57

85 5000

1 113 209 281 MMMMeMM /z-> —4 1111 100 50 ,1.... 150 — 200 250 300 350 400 450 35.40 35.60 35.80 36.00 m/ Z 71.10 79.74%

Au Abundance #311146: Octadecane, 3-ethyl-5-(2-ethylbutyl)- 43

71 5000 35.40 35.60 35.80 36.00 m/z 85.10 61.51%

m/z-> ‘ ' i 50 112— 183 100 150 • ■!>■■ 200 ■ 250 । 221 ■ 300 r . । , t 337 . । 350 i—i . . 400 । । । i i 450 | i

Abundance #355040: Dotriacontane F7 // A, / YAA.,A MA 35.40 35.60 35.80 36.00 5000 85 m/z 43.10 56.54%

■ ‘i . 1113.141, 106.... 281......... 422 450 m/z- > 50 100 150 200 250 300 350 400 450 Abundance #193178: Octadecane 57 35.40 35.60 35.80 36.00 m/z 99.10 27.05%

5000 85

~। . 1113,141. 169 197 254 .............................. ' 'I 1 '' ' ' I I ' ' ' TI 1 ' ' 1 i ' /z— > 50 100 150 200 250 300 350 400 450 35.40 35.60 35.80 36.00

00614.D SCAN508.M Wed Jan 30 09:02:16 2002 Page 14

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