GCMS analysis results for sample AD31639, Jan 28 2002

NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C: \MSDCHEM\1\5973N\02JAN17\31639.D Vial: 2 - Acq On : 17 Jan 2002 3:39 pm Operator: Sample : 508 scan Inst : Instrumen Mise : January 17, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C: \MSDCHEM\1. . . \SCAN508 .M (RTE Integrator) Title : 508 scan method 7 . — . Library : C:\DATABASE\WILEY7N.L &WUVV7 )‘6Px ********************************************************** y** * ** * * * * Peak Number 9 Docosane, 11-decyl- (CAS) $— Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T.

34.94 1.50 ug/L 688961 Perylene-dl2 34.42

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Docosane, 11-decyl- (CAS) $$ 11-... 451 C32H66 055401-55-3 90 2 Heneicosane $$ n-Heneicosane 296 C21H44 000629-94-7 87 3 Heptadecane, 9-octyl- 352 C25H52 007225-64-1 87 4 Docosane $$ n-Docosane $$ Normal... 310 C22H46 000629-97-0 87 Abundance Scan 2765 (34.942 min): 31639.D (-) m/z 57.10 100.00% 57

85 5000

1 ■ i ‘ ■ i • ■ ■ ■ i ' * ■ ■ i ■ ■ ■ ■ i 1 34.60 34.80 35.00 35.20 155 183 263 m/z 71.10 70.10% 0 ■ • i • "' | i > • IT’ i i i | । । । ■ | ■ i । i | ■ i । i p i । i | i r. H ।।। niz-> 40 60 80 1(» 120 140 160 180 200 220 240 260 280 3(X) 320 340 Abundance #355038: Docosane, 11-decyl- (CAS) $$ 11-n-Decyldocosane $... 57

%• 5000 ■ ■ /_____ _ i • ■ ■ ■ i ■ r ■ ■ i 1 ■ ■ 1 i • ■ • ■ i 1 85 34.60 34.80 35.00 35.20 m/z 43.05 57.45% 1 1′3.141169 197 225...................... oM 1 r | l 1rITru ‘I‘-TIr+t-las‘t1-i4"1t"**A88374048*2***I**AZ*| 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #245745: Heneicosane $$ n-Heneicosane 57 ■ ■ । ‘ । ■ T n 34.60 34.80 35.00 35.20 85 5000 .m/z 85.10 54.93%

0 113 141................. 288 296 .. ....... mlz—> Abundance 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 57 #300498: Heptadecane, 9-octyl- 34.60 34.80 35.00 35.20 7. m m/z 55.10 21.98%

5000 85

239 113.141 169 310 352 WWW miz—> Ouipanlyi 1 1 I I t _____________ 10′1′201111-1/1171922318107737 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 111+1141444* * “ ^ j1' ‘ ‘ I ‘ ‘ ‘ ‘ I ■ ■ ।11111" ■ ■ 14‘*114*i 34.60 34.80 35.00 35.20

31639.D SCAN508.M Tue Jan 22 08:37:09 2002 Page 11

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