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GCMS analysis results for sample AD31639, Jan 28 2002

Machine-extracted title · confidence 100%

Laboratory report showing GCMS analysis of sample AD31639 including unknown compounds and surrogate recovery data.

NYC-WTC_000049957–000049974

Folder label: “GCMS X 1/3/02 A 1/17/02

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NYC 9/11 Public Portal Document Library Search Compound Report Data, File : C:\MSDCHEM\1\5973N\02JAN17\31639.D Vial: 2 Acq On : 17 Jan 2002 3:39 pm Operator: Sample : 508 scan Inst : Instrumen Mise : January 17, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1. . .\SCAN5 08. M (RTE Integratory—7 Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ****************************************************************** * * * Peak Number 10 Hexacosane $$ n-Hexacosane Concentration Rank 5 R.T. EstConc Area Relative to ISTD R.T. 35.74 0.63 ug/L 288451 Perylene-d12 34.42 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Hexacosane $$ n-Hexacosane 366 C26H54 000630-01-3 91 2 Dotriacontane 451 C32H66 000544-85-4 91 3 Heneicosane $$ n-Heneicosane 296 C21H44 000629-94-7 90 4 Pentacosane $$ n-Pentacosane 352 C25H52 000629-99-2 90 Abundance Scan 2835 (35.741 min): 31639.D (-) m/z 57.10 100.00% 57

5000 85

35.40 35.60 35.80 '36.00' 11 0-T 112141 109..207 281................................................. m/z 71.10 64.06% z-> 50 100 150 200 250 300 350 400 450 Abundance #311169: Hexacosane $$ n-Hexacosane 57

5000 85 35.40 '35.6Q1 35.80 '36.00 ‘ ‘ ' m/z 43.10 49.33% 113,141 169 295 388 0-T I miz-> 50 100 150 200 250 300 350 400 450 Abundance #355040: Dotriacontane 57

35.40 35.60 35.80 36.00 5000 85 m/z 85.10 47.53%

0- ■ . hT 1141, i111 > i > ‘ 196 ........ 281 ,24° miz-> 50 100 150 200 250 300 350 400 450 Abundance #245745: Heneicosane $$ n-Heneicosane ‘48 । * » I • r • ’ | 57 35.40 35.60 35.80 36.00 m/z 99.10 20.05% 85 5000

0-1 113141 , 296 W IDAA—WAA n/z—> 50 100 150 200 250 300 350 400 450 35.40 35.60 35.80 36.00

31639.D SCAN508.M Tue Jan 22 08:37:10 2002 Page 12

NYC-WTC_000049972

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NYC-WTC_000049972Source: NYC Law Department, mirrored locally

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DEP GCMS data table, Jan-Feb 2002 · Box DEP Box 12

NYC-WTC_000003981

Multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.

1 shared non-person entities · 1 shared topics · similarity 0.994

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