GCMS analysis results for sample AE00614, Feb 2002

NYC 9/11 Public Portal Document

Library Search Compound Report . Data File : C:\MSDCHEM\1\5973N\02JAN29\00614 .D vial: 3 Acq On : 29 Jan 2002 4:17 pm Operator: Sample : 508 scan Inst : Instrumen Mise : January 29, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\l..-\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N. L ********************************************************************* Peak Number 9 Tetracosane Concentration Rank 11 R.T. EstConc Area Relative to ISTD R.T. 33.26 0.12 ug/L 86650 Perylene-dl2 34.42 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Tetracosane 338 C24H50 000646-31-1 53 2 Octacosane $$ n-Octacosane 394 C28H58 000630-02-4 53 3 Hexadecane 226 C16H34 000544-76-3 53 4 Octadecane, 2-methyl- 268 C19H40 001560-88-9 53 Abundance Scan 2618 (33.263 min): 00614. D (-) m/z 57.10 100.00% 57

5000 85

40 125 276 33.00 33.20 33.40 33.60 TVIBIBT 207 . ..... I........... .... T‘‘TTT‘TETETTTTTTTOTTETIT"T"TT i" " ।1 m/z 71.10 76.39% Tl/Z--> 40 60 80 100 120140160 180 200 220 240 260 280 300 320 340 360 380 Abundance #288784: Tetracosane 57

5000 85 AMaidMnM 33.00 33.20 33.40 33.60 m/z 43.05 48.18% 33 11 ■ । ■" ।1' j J 113 - 141 TTTUEmuT 197 225 294 338 r " ' i" " i" " i " "T ' " r " 11" '111 Wz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 Abundance #329266: Octacosane $$ n-Octacosane 57 MM ■ ■ i 1 33.00 33.20 33.40 33.60 5000 85 m/z 85.10 46.12%

m/z-> 171, 169 ,196 TI —utuu 224 “uuu-nmng 281 350 I" " I 394 TTr 40 60 80 100 120140 160 180 200 220 240 260 280 300 320 340 360 380 Abundance #154901: Hexadecane 57 33.00 33.20 33.40 33.60 m/z 99.10 21.10%

5000 85

I113 .. 226

m/z-> 1111 ■ ,4.4,4141 .... 196, i TT,,"l"”lllllllllll 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 I'1' ‘ I TCTTIUUpT 33.00 33.20 33.40 33.60

30614.D SCAN508.M Wed Jan 30 09:02:16 2002 Page 11

NYC-WTC_000051619