GCMS analysis results for sample AE00249, Jan 2002

NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\MSDCHEM\1\5973N\02JAN24\00249.D Vial: 5 Acq On : 24 Jan 2002 6:17 pm Operator: Sample : 508scan Inst : Instrumen Mise : January 24, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 10 Tetratriacontane $$ n-Tetra... Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T.

34.94 0.38 ug/L 227894 Perylene-d12 34.42

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Tetratriacontane $$ n-Tetratriac... 479 C34H70 014167-59-0 90 2 Pentatriacontane 493 C35H72 000630-07-9 90 3 Heneicosane (CAS) $$ n-Heneicosane 296 C21H44 000629-94-7 87 4 Octacosane (CAS) $$ n-Octacosane 394 C28H58 000630-02-4 86 Abundance Scan 2765 (34.941 min): 00249.D (-) m/z 57.10 100.00% 57

85 5000

113 il 130 11 in 207 263 34.60 34.80 35.00 35.20 ’ m/z 71.05 70.22% mfe-> 40 60 80 100120140160180200 220240260280300320340 360380400 Abundance #363627: Tetratriacontane $$ n-Tetratriacontane 57

5000 85 Cpvw .m 34.60 34.80 35.00 35.20 ' ' ' ' m/z85.10 55.65% 113.141 169 311 367 410 T-rp-rr TT — fl. ——11—I — t— 1 0000900 miz-> 40 60 80 100120140160180 200 220240260280300320340 360380 400

w ) Ms Abundance #367079: Pentatriacontane 57

34.60 34.80 35.00 35.20 5000 m/z 43.05 49.16% 85

| u113,141 , 169 197 225 “i'"' miz-> 40 60 80 100120140160180200220240260280300320340 360380400 Abundance #245747: Heneicosane (CAS) $$ n-Heneicosane * ' i • ■ • i ■ ■ ■ • i ■ ■ ■ • i 1

s 57 34.60 34.80 35.00 35.20 m/z 55.10 27.83%

5000' 85

I i 113 141 m/z-> "i"'pAkadaMoe 253 29.11.. . 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 400 34.60 34.80 35.00 35.20

00249.D SCAN508.M Fri Jan 25 10:26:18 2002 Page 12

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