GCMS analysis results for sample AD31639, Jan 28 2002

NYC 9/11 Public Portal Document Library Search Compound Report Data File : C: \MSDCHEM\1\5973N\02JAN17\31639.D Vial: 2 Acq On : 17 Jan 2002 3:39 pm Operator: Sample : 508 scan Inst : Instrumen Mise : January 17, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1.. .\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ************************************************************* *k****** Peak Number 6 Heptadecane $$ n-Heptadecan... Concentration Rank 6 R.T. EstConc Area Relative to ISTD R.T. 32.38 0.40 ug/L 221856 Chrysene-dl2 30.50 Hit# Of 5 Tentative ID MW MolForm CAS# Qual 1 Heptadecane $$ n-Heptadecane $$ ... 240 C17H36 000629-78-7 90 2 Heneicosane $$ n-Heneicosane 296 C21H44 000629-94-7 90 3 Octacosane $$ n-Octacosane 394 C28H58 000630-02-4 90 4 Octacosane (CAS) $$ n-Octacosane 394 C28H58 000630-02-4 86 Abundance Scan 2541 (32,384 min): 31639.D (-) m/z 57.10 100.00% 57

5000 85

AMANi -4- 155 32.00 32.20 32.40 32.60 32.80 207 0J v I r m/z 71.10 71.53% mz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 Abundance #174546: Heptadecane $$ n-Heptadecane $$ Normal-heptadecane 57

85 5000 44— 32.00 32.20 32.40 32.60 32.80 m/z 43.10 59.55% 0- "1“' 1,13,141.... 196... 240...................... niz—> 40 60 80 100120 140160 160 200 220 240 260 280 300 320 340 360 380 Abundance #245745: Heneicosane $$ n-Heneicosane 57 AMA N 85 32.00 32.20 32.40 32.60 32.80 5000 m/z 85.10 49.93%

n/z-> 0- Abundance 4 1113,141............... 268 296................ ! r.. . T.!. |. 111 j t...!.. I, (, I,, p .,. ].. r J J J11» p u 111J n | J1111J J111 U 11J M J JI r 40 60 80 100 120 140 1^)180 20)220 240 260 280 3(X) 320 340 360 380

57 #329266: Octacosane $$ n-Octacosane 1 T-[-r-r-n-p-r •• | • 32.00 32.20 32.40 32.60 32.80 m/ Z 55.10 28.53% 5000

1 0 TTp-rrr-p- 85

141,169196 113 224 281 350 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 394 .-j.... ।.. i*.... ].... ।,.,. ।.... 11. *. ।। < AAAAALIAA M 32.00 32.20 32.40 32.60 32.80

31639.D SCAN508.M Tue Jan 22 08:37:09 2002 Page 8

NYC-WTC_000049968