GCMS analysis results for sample AD31664, Jan 25 2002

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Laboratory report documenting GCMS analysis of sample AD31664 with detection of unknown compounds and surrogate recovery.

NYC-WTC_000050258–000050275

Folder label: “GCMS X 1/3/02 A 1/22 - 1/23/02”

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NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C:\MSDCHEM\1\5973N\02JAN22\31664.D Vial: 1 Acq On : 22 Jan 2002 2:41 pm Operator: Sample : 508 scan Inst : Instrumen Mise : January 22, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 10 5,5-DIMETHYL-1-PYRROLIN-2-Y... Concentration Rank 9

R.T. EstConc Area Relative to ISTD R.T.

38.96 0.04 ug/L 13803 Perylene-d12 34.42

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 5,5-DIMETHYL-1-PYRROLIN-2-YLMETH... 191 C7H13N03S 057625-16-8 5 N° 2 l-oxo-2,3,5,6,7,8-hexahydrothien... 207 C11H13NOS 109216-76-4 5 (=007 3 2-(N-Methylpyrrolyl) thienoate 207 C10H9NO2S 000000-00-0 5 MAC 4 3,5-Ethanoquinolin-10-one, decah... 207 C13H21NO 021041-42-9 5 Abundance Scan 3117 (38.960 min): 31664.D (-) m/z 207.00 100.00% 36 191 207 wWVwwwwh 49 5000

281 38.60 38.80 39.00 39.20 • ‘ i ■ • • ■ i ‘ ‘ ‘ ■ i ■ ■ i • ‘ ■ i • ■ ■ ■ i • ‘ ■ i • • • ■ i - m/z 96.00 77.94% n/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #101224:5,5-DlMETHYL-1-PYRROLIN-2-YLMETHANSULPHONIC ACID... 42 95 191 8000 82 55 111 6000 69 38.60 38.80 39.00 39.20 4000 m/z 191.00 77.21%

miz-> 2000- 40 ... 60 J801 . ।100 120 140 160 180 200 220 240 260 280 Abundance #125354:1-oxo-2,3,5,6,7,8-hexahydrothieno[2,3-b]quinoiine 191 207 ■ । ■ ‘*+14 ""1 i ■ 1 • 1 i ■ 38.60 38.80 39.00 39.20 5000 m/z 49.00 63.24% 163 139 A

■ • i ■ ‘ • i ' 1 • ‘ i ■ • ■ ■ i ' ■1 ' i ■ i ' ■ ‘ • i ‘ ‘ ■ i ■ iz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #125253: 2-(N-MethylpyrroIyl) thienoate 112 217 38.'60 38.80 39.00 39.2011 191 m/z 281.10 12.39% 5000 83 96 W W N L s A • 1 i1 * * * i • • • ’ i ' ’ ItT ‘ ‘ "41 । । । । । । . I1-r ’ • | ’ * * ′ | • m/z—> 40 60 80 100 120 140 160 180 200 220 240 260 280 38.60 38.80 39.00 39.20

31664.D SCAN508.M Thu Jan 24 14:00:07 2002 Page 12

NYC-WTC_000050273

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