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GC/MS analysis results for sample AE11416, May 28 2002

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Laboratory report documenting gas chromatography/mass spectrometry analysis of sample AE11416 conducted on May 28, 2002.

NYC-WTC_000025319–000025331

Folder label: “GCMS X 5/15/02 A 5/18/02

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Scanned page image, NYC-WTC_000025330
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NYC 9/11 Public Portal Document ULDLdLY DCdLCII wOIpOUI neyui L

Data File : C:\MSDCHEM\l\DATA\051702\11415.D Vial : 24 Acq On : 18 May 2002 8:21 am Operator: Mclean Sample : 5/15 eh Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\l\METHQDS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 5 Anthracene-dlO- Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T. 23.11 0.38 ug/L 377457 Phenant hranene - dl 0 22.95

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Anthracene-diO- 188 C14D10 001719-06-8 72 2 Phenanthrene-diO 188 C14D10 001517-22-2 72 3 Pentacyclo[7.3.1.1. (4,12) .0 (2,7) . .. 188 C14H20 1000215-61-8 38 4 1,4-Naphthalenedione, 2-hydroxy-... 188 C11H8O3 000483-55-6 9 Abundance Scan 3409 (23.109 min): 11415.D (-3402) (-) m/z 188.10 100.00% its

5000 -

40 0 ' i "111" " r ' " 111" i 66 80 94 156 I I’T 22.80 23.00 23.20 23.40 m/z 189.10 20.11% mfa-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #79826: Anthracene-d10- KS

5000 ... H.............. 22.80 23.00 23.20 23.40 m/z 94.10 13.15% 80 94 160 . . 66 17 30 42 52 108 118 132 146 I 170179 0 ' i " " r " ' i'' " i'1" i11' I 111 L I I d I I I I 11 I I | I I I I | r l ! ] I TTTTTTNTTTTTTTTTTTT mlz-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #79827: Phenanthrene-d10 188 ,... 22.80 23.00 23.20 23.40 5000 m/z 184.05 11.27%

80 94 160 30 42 52 66 108118 132 146 || 1701791,1 11 0- TTTTTTHTTPTTTTT h | I I I 1 | I ! I I | I I II j I I I I | H M | I I I I | I I l-i I I I I I ]

mfe-> 10 20 30 40 50 60 70 80 90 100110 120 130 140 150 160 170 180 190 Abundance #79715: Pentacyclo[7.3.1.1 .(4,12).0(2,7).0(6,11 )]tetradeca... ) 7‘T its 22.80 23.00 23.20 23.40 m/ Z 80.10 9.73% 5000- 79 91 55 67 131 145 159 173 105 117 n/z-> 0 4p 1 At,ll 1 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 ------- 22.80 23.00 23.20 23.40

11415.D 050102.M Tue May 21 15:57:55 2002 Page 7

NYC-WTC_000025330

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