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← Document results/DEP Box 18/GCMS X 5/15/02 A 5/18/02
Document / 12 pages

GC/MS data fragment, May 28 2002

Machine-extracted title · confidence 90%

Fragmented document containing GC/MS data from May 28, 2002.

NYC-WTC_000025332–000025343

Folder label: “GCMS X 5/15/02 A 5/18/02

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Scanned page image, NYC-WTC_000025342
OCR text

OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document UOLCLY DEdLCil woapOuIIU RCDOL L

Data File : C:\MSDCHEM\1\DATA\051702\11416.D Vial: 25 Acq On : 18 May 2002 9:10 am Operator: Mclean Sample : 5/15 eh Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C:\MSDCHEM\l\METHQDS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 4 Anthracene-dlO- Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 23.11 0.44 ug/L 392294 Phenanthranene-dl0 22.95 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Anthracene-diO- 188 C14D10 001719-06-8 87 2 2-Quinolinecarboxaldehyde , 8-hyd... 188 C10H8N2O2 005603-22-5 4/0 3 Phenanthrene-diO 188 C14D10 001517-22-2 38 4 Pentacyclo[8.4.0.0(3,7).0(4,14).... 188 C14H20 1000099-27-2 33 Abundance Scan 3409 (23.109 min): 11416.D (-3402) (-) m/z 188.10 100.00% 188

5000 94 ■ 1 i 1 ' 43 66 80 158 । 22.80 23.00 23.20 23.40 o', 111111111111 -H mmmmH ITT m/z 94.05 21.87% mfe-> 10 20 30 40 50 60 70 80 90 100110 120 130 140 150 160 170 180 190 Abundance #79826: Anthracene-d10- 188

5000 1 22.80 23.00 23.20 23.40 m/z 189.10 17.18% 80 94 160 , , 66 17 30 42 52 11111111 1 108 118 132 ......................................... 111 + TTTmTtm 0 TTTTmmummm’ir /z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #125696: 2-Quinolinecarboxaldehyde, 8-hydroxy-, oxime 188 Wn........... . 22.80 23.00 23.20 23.40 5000 m/z 184.00 14.17% 143 51 64l ' l'1 7641 1 ' I||89 । H >102 115 130 . , 158 170 | I P. . | . |ll na iIm, . . |‘ +H 0 qpomnqpmmnnpamnqpmndan miz-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance Phenanthrene-d10 .......... /................................... 1 ■ i ■ ' ■ ' i 1 1 ' ■ i 1 1 ' ' 1 1 1 1 ' I 188 22.80 23.00 23.20 23.40 m/z 80.00 11.81%

5000

80 94 160 30 42 52 66 11 108 118 132 146 |, 170179 - 0 TPWTTTTTTTTTTTTHmtutfTTTTTTTTT m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 22.80 23.00 23.20 23.40

11416.D 050102.M Tue May 21 15:58:27 2002 Page 6

NYC-WTC_000025342

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NYC-WTC_000025342Source: NYC Law Department, mirrored locally

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