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GCMS analysis results for sample AE11410, May 22 2002

Machine-extracted title · confidence 100%

Laboratory report showing GCMS analysis results for sample AE11410 conducted on May 22, 2002.

NYC-WTC_000025196–000025212

Folder label: “GCMS X 5/15/02 A 5/17/02

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Scanned page image, NYC-WTC_000025209
OCR text

OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document LLDLcLY DEdLtil topOuIIU RCPOL L

Data File : C:\MSDCHEM\1\DATA\051702\11409.D Vial: 12 Acq On : 17 May 2002 9:45 pm Operator: Mclean Sample : 5/15 ad Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 6 Anthracene-d10- Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T.

23.11 0.42 ug/L 456300 Phenanthranene-dl0 22.95

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Anthracene-diO- 188 C14D10 001719-06-8 72 2 Benzene, 1-(1-cyclohexen-l-yl) -4... 188 C13H160 020758-60-5 49 3 Phenanthrene-diO 188 C14D10 001517-22-2 45 4 Antipyrine 188 C11H12N20 000060-80-0 38 Abundance Scan 3409 (23.109 min): 11409. D (-3403) (-) m/z 188.10 100.00% 188

5000 94 -

mfe-> o > 111111 < । > 11 ■ 42 54 66 RR 80 1 1" i1"111 Hhp 1 fr rr+rri 111 I 1 I I I I I I I I I I I I I I I I I I I I I I

W 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 158 +n 22.80 23.00 23.20 23.40 m/ z 94.10 A 19.19% Abundance #79826: Anthracene-d10- 188

5000 22.80 23.00 23.20 23.40 m/z 189.20 18.60% 80 94 160 . . 17 30 42 52 66 108118 132 146> ,|,l 1701791,। I 0 —99,——]——————-HHH TINTmmmmutuHu TTTTT n/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #79791: Benzene, 1 -(1 -cyclohexen-1 -yl)-4-methoxy- 188 ................ ............ ........................ 22.80 23.00 23.20 23.40 5000 160 m/z 184.10 14.34%

115 129 145 173 41 51 65 77 ‘ 91|

miz-> 0 - 102 TTHT 10 20 30 40 50 60 70 80 90 100110 120 130 140 150 160 170 180 190 v A-n-nJ in ,-1'iL L Abundance #79827: Phenanthrene-d10 188 22.80 23.00 23.20 23.40 m/z 187.05 12.46%

5000

80 94 160 30 42 52 0 'I ""1111'I'11'I" "I11" I11,11" HI"1 66 11 108 118 132 146 •p-rrr -179179/— TT ' ■ i 1 ' 1 1 1 1 1 1 1 I ' ' ' ' I /z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 22.80 23.00 23.20 23.40

11409.D 050102.M Tue May 21 11:57:11 2002 Page 9

NYC-WTC_000025209

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NYC-WTC_000025209Source: NYC Law Department, mirrored locally

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