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GCMS analysis results for sample AE11410, May 22 2002

Machine-extracted title · confidence 100%

Laboratory report showing GCMS analysis results for sample AE11410 conducted on May 22, 2002.

NYC-WTC_000025196–000025212

Folder label: “GCMS X 5/15/02 A 5/17/02

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NYC 9/11 Public Portal Document LLDLdLy bedrCI copourd Report Data File : C:\MSDCHEM\1\DATA\051702\11409.D Vial: 12 Acq On : 17 May 2002 9:45 pm Operator: Mclean Sample : 5/15 ad Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 5 2,4-Diamino-6-(hydroxymethy... Concentration Rank 5 R.T. EstConc Area Relative to ISTD R.T.

22.58 0.27 ug/L 295328 Phenanthranene-dlO • 22.95

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2,4-Diamino-6-(hydroxymethyl)pte... 192 C7H8N60 000945-24-4 59 2 1,5-Naphthalenedithiole 192 C10H8S2 1000223-69-5 38 3 2-Imidazolidinone, 1-methoxy-3-p... 192 C10H12N2O2 052420-43-6 38 4 Phenanthrene, 3-methyl- 192 C15H12 000832-71-3 36 Abundance Scan 3319 (22,580 min): 11409.D (-3311) (-) -m/z 192.10 100.00% 192

5000

- 62 96 146 160 22.20 22.40 22.60 22.80 23.00 mlz-> 120 O-pmmmHptTTTPT 49 70 HH “ | I— 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 m/z 191.00 fl 17.86%| Abundance #80958: 2,4-Diamino-6-(hydroxymethyl)pteridine 43 163 192

5000 — 22.20 22.40 22.60 22.80 23.00 28 53 68 146 176 m/z 146.10 16.36%| 77 92 106 121 133 0 "I‘ +l-44/4+4ll p-TT - m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #80950: 1,5-Naphthalenedithiole 192 ..... 1 22.20 22.40 22.60 22.80 23.00 5000 m/z 96.00 13.88% 115 128 159 40 57 69 79 96 . 147 177 ot ---------- - 11T'1 I'1 ‘ ITT n/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #80907: 2-lmidazolidinone, 1 -methoxy-3-phenyl- 106 192 22.20 22.40 22.60 22.80 23.00 m/z 193.00 12.61%| 77 119 162. 5000 42 56 91

n/z-> 0 28 —4HH I । Anil'll I h " " i"1111 1. ■ ■ ■ ■ i ■ I ■ ■ 11" ■ i ■ ■ • ■ | i

20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 134 "' ।" " ।11" । "' i" ...... I!.... H. 22.20 22.40 22.60 22.80 23.00

11409.D 050102.M Tue May 21 11:57:09 2002 Page 8

NYC-WTC_000025208

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NYC-WTC_000025208Source: NYC Law Department, mirrored locally

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