GCMS quantitation report, May 22 2002

NYC 9/11 Public Portal Document Library Search compound. Report Data File : C:\MSDCHEM\l\DATA\052202\11905.D Vial: 12 Acq On : 22 May 2002 10:47 pm Operator: Mclean Sample : 5/21 ad Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\052202.M (Chemstation Integrator) Title : 508 Modified GC/MS scan *• Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 14 Phenanthrene-diO Concentration Rank 11 R.T. EstConc Area Relative to ISTD R.T. 23.07 0.29 ug/L 335992 Phenanthranene-dl0 22.92 Hit# of 5 Tentative ID MW MolForm CAS# Qual A 1 Phenanthrene-diO 188 C14D10 001517-22-2 83 y 2 Anthracene-diO- 188 C14D10 001719-06-8 530 3 4-Methyl-2-(4-fluorophenyl)pyrim... 188 C11H9FN2 076128-67-1 40 4 Imidazole, 4-carboxy-5-phenyl- 188 C10H8N2O2 1000116-63-8 37 Abundance Scan 3402 (23.068 min): 11905.D (-3396) (-) m/z 188.10 100.00% 188

5000

80 94 160 43 57 66 22.80 23.00 23.20 23.40

n/z-> 0 ■| nj..... ■ 11' ■' 11 ■ ■ 11'.'.. ■ ।.., u l. |'i. 11 , TT 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 I ll “ I ■' m/z 94.05 17.22% Abundance #79827: Phenanthrene-d10 188

5000 22.80 23.00 23.20 23.40 m/ z 80.00 14.28% 80 94 160 /J 30 42 52 66 , 0 T 11 Fr "111'1 11111 i 11 l i 111 ri 11111H 1111 108118 132 TT^H-I.[|||I|.I||||.|.|||| Tn I 146—4170179 mfe-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #79826: Anthracene-d10- 188

22.80 23.00 23.20 23.40 5000 m/z 184.10 11.73%

17 30 42 52 ° 80 | 94 108118 132 146 1 160 170179, 0-'> | H ■ ■ | I I I I J I H I ) I I > 1 | I t ■ I | H I I | H t I 11 I . 1 | I I . . [ I I . . [ ■ . 1 I [ . ■ , , Tl-T t . J l ■ » . [ | I ■ ? iJTl’ll i i . m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #79745:4-Methyl-2-(4-fluorophenyl)pyrimidine 188 22.80 23.00 23.20 23.40 m/z 160.10 11.20% 121 5000 173 . 67 94 . 184 |, | 133 146 161 ___ । 0 ‘ i " “ i ■ " ‘ i ■ ■'39 11 •1 ■ ■ I ' 57i'1,1| 111,11 11111111 ''11111111" | —————— h.. n/z-> 10 20 30 40 50 60 70 80 90 100110 120 130 140 150 160 170 180 190 22.80 23.00 23.20 23.40

11905.D 052202.M Tue May 28 12:12:19 2002 Page 17

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