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GCMS analysis results for sample AE11410, May 22 2002

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Laboratory report showing GCMS analysis results for sample AE11410 conducted on May 22, 2002.

NYC-WTC_000025196–000025212

Folder label: “GCMS X 5/15/02 A 5/17/02

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NYC 9/11 Public Portal Document Licrary searcn compound Report

Data File : C:\MSDCHEM\1\DATA\051702\11409.D Vial: 12 Acq On : 17 May 2002 9:45 pm Operator: Mclean Sample : 5/15 ad Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L

Peak Number 7 6-Methylamino-2-phenyl-1,3. Concentration Rank 8

R.T. EstConc Area Relative to ISTD R.T.

31.04 0.20 ug/L 176152 Chrysene-dl2 30.81

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 6-Methylamino-2-phenyl -1,3,5-thi... 235 C10H9N3S2 094014-49-0 5/ 2 l-Cyano-3-methyl-cyclohexa-1,3-d... 119 C8H9N 1000145-23-0/5 3 Dimethylphosphinic azide 119 C2H6N30P 058347-13-0/4 4 5-(Ethoxycarbonylmethylene)cyclo ... 239 C13H21NO3 1000106-1142 4 Abundance Scan 4758 (31.035 min): 11409.D (-4757) (-) m/z 106.10 100/. 00% 106

117 208 5000 235 44

30.80 31.00 31.20 31.40 O+ ’1’’I ' ’ ' I ' ' ' 1 I ‘ ' I ■ * i * ■ • * i 1 ■ 1 ■ i ■ 1 • ■ r* * * * । * m/z 104.10 64.97% miz-> 20 40 60 80 100 120 140 160 180 200 220 240 Abundance #45216: 6-Methylamino-2-phenyl-1,3,5-thiadiazine-4-thione 104

235 5000 30.80 31.00 31.20 31.40 77 m/z 2 08.10 53.29% 51| 01 --------- 40 | I 132 149 ‘3 177 202......, ' ' I ' 1 1 ' 1 1 ' ‘ ' I ' ' 1 ' I ' ' 1 1 1 1 ' ' 1 I ‘ ' 1 1 I 1 1 miz-> 20 40 60 80 100 120 140 160 180 200 220 240 Abundance #45047:1 -Cyano-3-methyl-cyclohexa-1,3-diene 104 119 30.80 31.00 31.20 31.40 5000 m/z 117.20 52.10% 91

01 m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 Abundance #6694: Dimethylphosphinic azide TT I....... ' I ' ‘ 1 ‘ I 1 ' 28 43 77 30.80 31.00 31.20 31.40 m/z 235.10 47.31%

5000 119 104 15 0 1_ 159 . ' 1 1 1 ' I ' ' 1 1 I ' 1 1 ' I ' ' I ' 1 I ' ' 1 1 I 1 1 /z-> 20 40 60 80 100 120 140 160 180 200 220 240 30.80 31.00 31.20 31.40

11409.D 050102.M Tue May 21 11:57:14 2002 Page 10

NYC-WTC_000025210

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NYC-WTC_000025210Source: NYC Law Department, mirrored locally

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