GCMS blank analysis results for sample AE00327, Jan 2002

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Laboratory report documenting GCMS blank analysis to verify system cleanliness during January 10-11, 2002 testing.

NYC-WTC_000051179–000051191

Folder label: “GCMS X 1/8/02 A 1/10/02”

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NYC 9/11 Public Portal Document

Llprary searcn compound Report

Data File : C:\MSDCHEM\l\5973N\02JAN10\0108B.D Vial: 1 Acq On : 10 Jan 2002 12:21 pm Operator: Sample : lab blank ext 1/8 Inst : Instrumen Mise : January 10, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\l..-\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L

Peak Number 6 4-METHOXY-.BETA.-METHYLCINN. .. Concentration Rank 4 R.T. EstConc Area Relative to ISTD R.T. 22.28 0.14 ug/L 73216 Phenanthrene-dl0 22.65 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 4-METHOXY-.BETA.-METHYLCINNAMIC ... 192 C11H12O3 019169-94-9 72 2 Phenanthrene, 9-methyl- $$ 9-Met... 192 C15H12 000883-20-5 59 3 2,4-Diamino-6-(hydroxymethyl)pte... 192 C7H8N6O 000945-24-4 59 4 Phenanthrene, 2-methyl- 192 C15H12 002531-84-2 53 Abundance Scan 1656 (22.280 min): 0108B.D (-) m/z 192.10 100.00%) 192 A 5000 ................... .......................... 146 66 82 118 f 160 II 22.00 22.20 22.40 22.60 Ot < I' ■1 ‘ I44 '1 ■ ’ i ‘ -PH —P "Ip .................. 1 .... I........... ll TT‘ m/z 146.10 18.38% m/z-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #102588: 4-METHOXY-.BETA.-METHYLCINNAMIC ACID $$ 2-Butenoi... 192

5000- 108 ।''' T A ) 22.00 22.20 22.40 22.60 146 175 m/z 191.10 16.25% 0 I h I” '’ I' ‘ '1 I " " I " ‘' I ” '' I I " 1' 1 I ''1' I' " ' 11''11 I " " I " ‘ I' r " 11 m/z-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #103936: Phenanthrene, 9-methyl- $$ 9-Methylphenanthrene 192 1 ■ i • ’ ■ ■ i 1 ■ ■ ■ i ■ 1 । ■ 1

22.00 22.20 22.40 22.60 5000 m/z 193.10 14.52%

96 165 88 l 139 152 176 0 "| — TTTTT | 1 1 • | '^Tp' i i । i i i i । i n f । । I I । । । ! । । । । । । । । । । । i । i । । i'| ) i r r । t TTT TT" mfz-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #102010:2,4-Diamino-6-(hydroxymethyl)pteridine ...................................... , 192 22.00 22.20 22.40 22.60 163 m/z 96.00 13.49% 5000

66 146 175 121I 135 0 34 TWTTTTTT TT 11'' ‘ I " 1' I ‘'1' I •''11 " 1' 11 " ' 11'1111 I -ll TI1" m/z-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 22.00 22.20 22.40 22.60

108B.D SCAN508.M Fri Jan 11 10:09:15 2002 Page 8

NYC-WTC_000051189

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NYC-WTC_000051189Source: NYC Law Department, mirrored locally

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GCMS analysis results for sample AE00309, Jan 2002 · Box DEP Box 28

NYC-WTC_000051088

Laboratory report showing GCMS analysis of sample AE00309 for unknown compounds and DDD on January 10, 2002.

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