GCMS analysis results, sample AE12322, June 2002

NYC 9/11 Public Portal Document Library searcn compound Report Data File : C:\MSDCHEM\l\DATA\052902\12322.D Vial: 10 Acq On : 29 May 2002 5:25 pm Operator: McLean Sample : gc/ms scan 5/24 Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\052202.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 10 Phenanthrene, 9-methyl- Concentration Rank 11 R.T. EstConc Area Relative to ISTD R.T. 22.54 0.27 ug/L 258497 Phenant hranene - dl 0 22.91 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Phenanthrene, 9-methyl- 192 C15H12 000883-20-5 53 2 1H-2-Indenone,2,4,5,6,7,7a-hexah. . . 192 C13H20O 1000196-69-5 4 3 Anthracene, 9-methyl- 192 C15H12 000779-02-2 40 4 Anthracene, 2-methyl- 192 C15H12 000613-12-740 Abundance Scan 3311 (22.533 min): 12322.D (-3300) (-) m/z 192.10 100.00% 192

5000

82 96 146 160 , 42 52 70 | I 22.20 22.40 22.60 22.80 118 01 q i i 1 ■ | ■ ■ 1 ij I 1 ■ i'| 11 i i fT-i 11 ] i i II | 111 i j 11 11 । i > I IIWPPI mH - m/z 193.00 15.88% m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #81033: Phenanthrene, 9-methyl- 192 — 5000 TI 22.20 22.40 22.60 22.80 m/z 146.10 15.66% 29 39 51 63 74 83 * 115 126 139 152 165 176 | 0! ‘ 1 1 " ‘ I ‘ " ‘1 ‘ ' I " ' ‘ 1 ' " • i ' ■ rH rirl lj l > V l p >■> l | > vu | 1 l > >'| 1 U I p I 1 1 | ih'lTj l ri | 1 ! ’ -rrp-r iz-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #80945: 1 H-2-Indenone,2,4,5,6,7,7a-hexahydro-3-(1-methylet... 192 149 22.20 22.40 22.60 22.80 177 5000 m/z 82.00 15.10% 41 93 107 121 135 164 55 67 79 27 0- + M+4HHIHlH4lHH+** H l U’T miz-> 20 30 40 50 60 70 80 90 100110120130140150160170180190200 Abundance #125848: Anthracene, 9-methyl- 192 PAm / \ ‘ I ‘ ‘ 22.20 22.40 22.60 22.80 ' I

m/z 191.00 14.87%

5000

96 P 27 39 51 63 82 II 115 126 139 152 19 176 „I 0 i j-«*** 11 i t ry > 11 > |* 1111 Tii 11 k j"i» [TTTp r 111' 111 j 11 j i’i i j 111‘11111’* 11111*1'1 j j rttT rrfi ।1 j । lip ! i j j j r mfa-> 2030405060 70 8090 100 110120 130140 150 160 170 180 190 200 22.20 22.40 22.60 22.80

12322.D 052202.M Mon Jun 03 10:49:51 2002 Page 13

NYC-WTC_000014277