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GCMS analysis results, sample AE12322, June 2002

Machine-extracted title · confidence 100%

Gas chromatography mass spectrometry results for sample AE12322 including surrogate recovery data analyzed on June 7, 2002.

NYC-WTC_000014260–000014280

Folder label: “GCMS X 5/24/02 A 5/29/02

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NYC 9/11 Public Portal Document • -L CL Y DarcIl toLpourC KCpOIC

Data File : C:\MSDCHEM\1\DATA\052902\12322.D Vial: 10 Acq On : 29 May 2002 5:25 pm Operator: McLean Sample : gc/ms scan 5/24 Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\052202.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L

Peak Number 11 Anthracene -d10- Concentration-Rank 9

R.T. EstConc Area Relative to ISTD R.T. 23.07 0.28 ug/L 268507 Phenanthranehe-dl0 22.91 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Anthracene-dlO- 188 C14D10 001719-06-8 78 2 Phenanthrene-diO 188 C14D10 001517-22-2 72 3 Pentacyclo[7.3.1.1. (4,12) .0 (2,7) ... 188 C14H20 1000215-61-8 45 4 4-Methyl-2-(4-fluorophenyl)pyrim... 188 C11H9FN2 076128-67-1 38 Abundance Scan 3402 (23.068 min): 12322.D (-3396) (-) m/z 188.10 100.00%| 188

5000 ........................ .. 80 94 160 । 22.80 23.00 23.20 23.40

niz-> 0 T71----H 40 49 MTTTTTT 66 . 132 T’T 10 20 30 40 50 60 70 80 90 100110 120 130 140 150 160 170 180 190 -H rn/z 189.10 19.69%I Abundance #79826: Anthracene-d10- 188

- 5000 22.80 23.00 23.20 23.40 m/z 80.00 17.76% 160 , 17 30 42 52 4 6 * —108118.132.1464179179,— 0 ' i ■ ■ ■ ■ i11 ■ ■ i1 ■ 11111111111 > । rl I >[ i rHti 1i " Tifa-> 10 2030405060 70 8090 100110120130140150160170180190 Abundance #79827: Phenanthrene-d10 188

22.80 23.00 23.20 23.40 5000 m/z 184.10 15.34%|

94 80 160 30 42 52 11 66 . 108118 132 146 , |,| 1701791, | 0 ■I “ I ■ “ 11111111U1111 “ 11I [ 11 H11111 ] 11.1 [ 11 n 11,. i-|: H i |I ■ 1.11, f. j, rl'l'l’... ., ■, । i'1'l TTpr miz-> 10 20 30 40 50 60 70 80 90 100110120130140150160170180190 Abundance #79715: Pentacycb[7.3.1.1.(4,12).0(2,7).0(6,11)]tetradeca... 188 22.80 23.00 23.20 23.40 m/z 94.10 14.94%

5000 79 91 55 67 105 117 131 145 159 0 mmmPpTp 173 WTPmaar 1 mhm miz-> 10 2030405060 70 8090 100110120130140150160 170 180 190 22.80 23.00 23.20 23.40

12322.D 052202.M Mon Jun 03 10:49:53 2002 Page 14

NYC-WTC_000014278

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NYC-WTC_000014278Source: NYC Law Department, mirrored locally

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