GCMS analysis results, sample AE12325, June 2002

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Data File : C:\MSDCHEM\l\DATA\052902\12325.D Vial: 13 Acq On : 29 May 2002 7:51 pm Operator: McLean Sample : gc/ms scan 5/24 Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\052202.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DAT7kBASE\NIST98.L

Peak Number 9 Anthracene-dlO- Concentration Rank 7

R.T. EstConc Area Relative to ISTD R.T.

23.07 0.31 ug/L 330990 Phenant hranene - dl 0 22.91

Hit# of 5 Tentative ID MW MolForm CAS# Qu 1 Anthracene -d10- 188 C14D10 001719-06-8 87 2 Phenanthrene-diO 188 C14D10 001517-22-2 83 3 4-Methyl-2-(3-fluorophenyl)pyrim... 188 C11H9FN2 076128-66-0 50 4 4-Methyl-2-(4-fluorophenyl)pyrim... 188 C11H9FN2 076128-67-1 38 Abundance Scan 3402 (23.068 min): 12325.D (-3395) (-) m/z 188.10 100.00% 118

5000

80 94 160 22.80 23.00 23.20 23.40 43 . - 66 - 132 146 1 0-+7111+ ‘1 1 m/z 184.10 19.61% ~n!z~> 10 20 30 40 50 60 70 80 90 100110 120 130 140 150 160 170 180 190 Abundance #79826: Anthracene-d10- 1t8

- 5000 22.80 23.00 23.20 23.40 m/z 94.10 13.19% 80 94 _ 180 miz-> 17 0 TTTTTIHt 30 42 52 66 . 108118 132 146 11. 170179, TWTmtt 10 2030405060 70 8090 100110120130140150160170180190 I Abundance #79827: Phenanthrene-d10 188

22.80 23.00 23.20 23.40 5000 m/z 80.00 13.16%

80 94 160- 30 42 52 66 0 rgmnapeimonattuni"i i >rii f.।.i l-l f i .> i ] +++198.118—.132,146+4179179l—.. "T mfe-> 10 20 30 40 50 60 70 80 90 100110120130140150160170180190 Abundance #79744:4-Methyl-2-(3-fluorophenyl)pyrimidine 1 Ai । in । । । i US 22.80 23.00 23.20 23.40 m/z 189.20 12.95%

5000 121

173 67 94 39 50 | , 82 |, 108 134 146161 I. I 0TIYaBAyeanguaahehusth |‘i! 111'T'l i > 11111 j i 111 |‘l ri > ["i 111I—BI—0-790111114111 n .-| IBUII541i ““i m/z—> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 22.80 23.00 23.20 23.40

12325.D 052202.M Mon Jun 03 10:53:25 2002 Page 12

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