GCMS analysis results, sample AE12325, June 2002

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Gas chromatography mass spectrometry results for sample AE12325 including surrogate recovery data analyzed on June 7, 2002.

NYC-WTC_000014330–000014347

Folder label: “GCMS X 5/24/02 A 5/29/02”

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NYC 9/11 Public Portal Document LLJLCLX DEaLtL totpOULU RCDOLL

Data File : C:\MSDCHEM\1\DATA\052902\12325.D Vial: 13 Acq On : 29 May 2002 7:51 pm Operator: McLean Sample : gc/ms scan 5/24 Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\052202.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 8 2,5-Dihydrophosphole, 3-met... Concentration Rank 8 R.T. EstConc Area Relative to ISTD R.T.

22.54 0.26 ug/L 279725 Phenanthranene- dl 0 22.91

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2,5-Dihydrophosphole , 3-methyl-l... 192 C11H130P 1000196-97-5/59 2 Anthracene, 2-methyl- 192 C15H12 000613-12-7/59 3 1,2-Phenylene diisothiocyanate 192 C8H4N2S2 071105-17-4 42 4 Bitoscanate 192 C8H4N2S2 004044-65/9 40 Abundance Scan 3312 (22.539 min): 12325.D (-3305) (-) m/z 192.10 0.00% 192

5000 ........... /M 36 70 82 j6 118 146 160 160 1 22.20 22.40 22.60 22.80 0- i।।. J , |।p. 11111 < I111 j।11।‘ j|।।. I'll >. 11 . m/z 191.10 24.82% miz-> 0 10 20 30 40 50 60 70 80 90 100110120130140150160170180190200 Abundance #80965:2,5-Dihydrophosphole, 3-methyl-1-oxo-1-phenyi- 192 164

5000 99 115 22.20 22.40 22.60 22.80 47 77 177 m/z 146.10 15.07% 67 125 146

miz-> 0 ‘‘**41 Tm 2737 54 ,57 h +++874+4+r4.39,+44+——77 HH ‘rrryrr 0 1020304050607080 90100110120130140150160170180190200 Abundance #125847: Anthracene, 2-methyl- 192 .A 22.20 22.40 22.60 22.80 5000 m/z 96.10 12.55%

28 39 51 63 82 96 115 126 139 152 165 176 0- TImTWTCTTTTTTTTTTTITTTTTTTHT ‘ITT miz-> 0 1020304050607080 90100110120130140150160170180190200 Abundance #80862:1,2-Phenylene diisothiocyanate 192 22.20 22.40 22.60 22.80 m/z 193.10 12.44% 64 5000

39 50 । 75 90 134

m/z—> 0 —418 4+.++ I 1 107 122 . 148 160 HHhttthhpnpptmmp 0 10 20 30 40 50 60 70 80 90 100110120130140150160170180190200 ' ■ i ■ ' ' ■ i 1 ' ■ ' i ■ ■ ' ' i ‘ 1 1 • i 22.20 22.40 22.60 22.80

12325.D 052202.M Mon Jun 03 10:53:24 2002 Page 11

NYC-WTC_000014345

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