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GCMS analysis results, sample AE12322, June 2002

Machine-extracted title · confidence 100%

Gas chromatography mass spectrometry results for sample AE12322 including surrogate recovery data analyzed on June 7, 2002.

NYC-WTC_000014260–000014280

Folder label: “GCMS X 5/24/02 A 5/29/02

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NYC 9/11 Public Portal Document ULDLCLY DCaLCL woLpOULC KCDOL L

Data File : C:\MSDCHEM\1\DATA\052902\12322.D Vial: 10 Acq On : 29 May 2002 5:25 pm Operator: McLean Sample : gc/ms scan 5/24 Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\052202.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 12 4-Octene, (E)- Concentration Rank 12 R.T. EstConc Area Relative to ISTD R.T. 33.79 0.25 ug/L 91523 Perylene-dl2 34.65 Hit# of 5 Tentative ID MW MolForm CAS# Qua

1 4-Octene, (E)- 112 C8H16 014850-23-8/27 2 4-Octene, (E)- 112 C8H16 014850-23-8 27 3 Decane, 3,4-dimethyl- 170 C12H26 017312-45-7 27 4 4-Octene, (E)- 112 C8H16 014850-23-8 22 Abundance Scan 5227 (33.791 min): 12322.D (-5222) (-) m/z 185.10 /OO.00% 116 57 43 71 5000 112 83 98 207 33.40 33.60 33.80 34.00 34.20 1111 1111 ■ n 11 '.| I H ! 11 J

nfe-> 0 .. |... 1... i“"i 10 20 30 40 50 60 70 80 90 100110120130140150160170180190200210 m/z 57.20 73.01% Abundance #111302:4-Octene, (E)- 41 55

- 5000 70 33.40 33.60 33.80 34.00 34.20 27 83 112 m/z 55.10 70.24%

n/z-> 0- nprpmtm 15 MlMtmHpm "‘l11121111151:1111111111137117011110301321013T 10 20 30 40 50 60 70 80 90 100110120130140150160170180190200210 Abundance #13070:4-Octene, (E)- 55 41 33.40 33.60 33.80 34.00 34.20 5000 70 m/z 71.10 59.76% 83 112 27 ........ 1, I . I'. ........ 0 1’1’1110900100080332111111 ‘‘‘I992111031213211111"152771E1"1911199381T"T7‘1‘3T tnfe-> 10 20 30 40 50 60 70 80 90 100110120130140150160170180190200210 Abundance #16527: Decane, 3,4-dimethyl- 57 33.40 33.60 33.80 34.00 34.20 43 m/z 70.10 57.59% 71 5000

29 85 112 J. ill 99 |, 127 141151 170 0-p j ... T ,,, l, |, i . I I'l.. (, 1111111'| 1111 m 11 rri 1111 n 11111111 u I ■ n 111 u ,,,,,,,,,, ,i, miz—> 10 20 30 40 50 60 70 80 90 100110120130140150160170180190200210 33,40 33.60 33.80 34.00 34.20

12322.D 052202.M Mon Jun 03 10:49:55 2002 Page 15

NYC-WTC_000014279

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NYC-WTC_000014279Source: NYC Law Department, mirrored locally

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