GCMS data file header for May 24-28, 2002

NYC 9/11 Public Portal Document Llbrary searcn compound Report Data File : C:\MSDCHEM\1\DATA\052802\524LB.D Vial: 3 Acq On : 28 May 2002 3:56 pm Operator: McLean Sample : 5/24 ad Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\052202.M (Chemstation Integrator) Title : 508 Modified GC/MS scan ** Library : C: \DATABASE\NIST98 . L ********************************************************************* Peak Number 10 Phenanthrene-diO Concentration Rank 15 R.T. EstConc Area Relative to ISTD R.T. 23.07 0.30 ug/L 292215 Phenanthranene - dl 0 22.91 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Phenanthrene-diO 188 C14D10 001517-22-2 64 2 Anthracene-d10- 188 C14D10 001719-06-8 47 3 Antipyrine 188 C11H12N2O 000060-80-0 40 4 Antipyrine 188 C11H12N2O 000060-80-0 40 Abundance Scan 3402 (23.068 min): 524LB.D (-3394) (-) m/z 188.10 100.00% 188

5000

94 80 22,80 23.00 23.20 23.40 43 I 66 57 ■ 160 178 0- I | I . L I1! > i l | I | > 1 | > , 1 TLWTNNTTTPTNITTTITT m/z 94.00 20.57% niz-> 10 20 30 40 50 60 70 80 90 100110 120 130 140 150 160 170 180 190 Abundance #79827: Phenanthrene-d10 188

5000 22.80 23.00 23.20 23.40 80 m/z80.10 13.20%| 94 160 30 42 52 66 . 11 108118 132 146 11 170179 0 'i 1111111 > i r| n > i fl 111111111 rl I > 111 !■! i TTTTTITTTTTTTTT niz-> 10 2030405060 70 8090 100110120130140150160170180190 Abundance #79826: Anthracene-d10- 188 /................................

22.80 23.00 23.20 23.40 5000 m/z 184.00 12.64

80 94 160 17 30 42 52 0 108118 132 146 r|| 1701791 al 0 9— TTHNtmmt Vttt m/z-> 10 2030405060 70 8090 100110120130140150160170180190 .... Abundance #125690: Antipyrine 188 22.80 23.00 23.20 23.40 m/z 189.10 12.06 96 5000 77 56 105 43 1 67 115 129 159 1/3 , 0 ----+---+-A-l-4++4pl mmmm TTTTT •n/z-> 10 20 30 40 50 60 70 80 90 100110 120 130 140 150 160 170 180 190 22.80 23.00 23.20 23.40

524LB.D 052202.M Thu May 30 10:44:17 2002 Page 13

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