GCMS data file header for May 24-28, 2002

NYC 9/11 Public Portal Document LLVLcLY bedrCI totpouu KepOLL

Data File : C: \MSDCHEM\ 1 \DATA\ 052802\524LB.D Vial: 3 Acq On : 28 May 2002 3:56 pm Operator: McLean Sample : 5/24 ad Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\052202.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L

Peak Number 11 1-Hexacosanol Concentration Rank 4 R.T. EstConc Area Relative to ISTD R.T. 28.96 1.29 ug/L 1011310 Chrysene-dl2 30.76 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 1-Hexacosanol 382 C26H540 000506-52-5 74 2 l-Dotriacontanol 467 C32H660 006624-79-9 70 3 1-Tetracosanol 354 C24H50O 000506-51-4/62 4 1-Docosene 308 C22H44 001599-67-3 62 Abundance Scan 4405 (28.961 min): 524LB.D (-4395) (-) m/ z 55.10 100.00% 55

5000 83

, 111 28.60 28.80 29.00 29.20

niz-> 0- 0 -450 Il,410044141 150 207 200 250 300 350 400 450 m/z 43.10 54.86% Abundance #109608: 1-Hexacosanol 43

5000 83 —A4IY*44-410 28.60 28.80 29.00 29.20 18 m/z 57.10 52.52% 111 044 r il 1 ,139 168 196 224 252 278 308 336 364 11d0mmmLTmTTTOTT niz-> 0 50 100 150 200 250 300 350 400 450 Abundance #16786:1-Dotriacontanol . . n 244 57 83 28.60 28.80 29.00 29,20 5000 m/z 83.10 46.63% 111

0- 111 1139-167-196,222 250 278,306, . 348 ’I’ 376 ■ * i 420 446 ■ 1 **u ■ ■ miz-> 0 50 100 150 200 250 300 350 400 450 Abundance #5175:1-Tetracosanol ----- 43 28.60 28.80 29.00 29,20 m/z 73.10 41.70% 5000 83

18 il 111 0- 41444,44.. i 1BatrI**/d 266 +1*I**I*!* 1140 168 198 238 ’ 308 336 n/z-> 0 50 100 150 200 250 300 350 400 450 28.60 28.80 29.00 29.20

524LB.D 052202.M Thu May 30 10:44:18 2002 Page 14

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