GCMS analysis results, sample AE11797, May 2002

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\MAY2102\117 97.D Vial: 38 Acq On : 23 May 2002 3:03 am Operator: Sample : EXTRACTS/20 Inst : 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0520.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L Peak Number 2 l-Dotriacontanol Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 31.11 0.99 ug/1 50467 Chrysene-dl2 33.57 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 1-Dotriacontanol 467 C32H660 006624-79-9 64 2 1-Tetracosanol 354 C24H50O 000506-51-4 58 3 1-Hexacosanol 382 C26H540 000506-52-5 53 4 Phosphonic acid, dioctadecyl ester 587 C36H7503P 019047-85-9 53 Abundance Scan 2845 (31.110 min): 11797.D (-) m/z 55.10 100.00%| 55

5000 83 111 30,80 31,00 31.20 31.40 r m/z 57.10 65.44% m/z-> 50 100 150 200 250 300 350 400 450 Abundance #57795: 1-Dotriacontanol 57

5000 83

111 L 30.80 31.00 31.20 31.40 m/z 43.10 64.95%

1 1 I 50 —4142, 100 150 196 420 448 ' i ' ' ' ' i 1 ' ' ' i ' 1 ' ' i ■ ' ' ‘ i ' ' ' ■ i ■ 200 250 300 350 400 450 Abundance #49775:1-Tetracosanol 43

30.80 31.00 31.20 31.40 5000 83 m/z 69.05 46.89%

111 H , 308 336 ■ 1 1 miz-> 50 100 150 200 250 300 350 400 450 Abundance #52385:1-Hexacosanol 43 30.80 31.00 31.20 31.40 m/z 73.10 44.66% 5000 83

111 I a),... ... ..... 364 -4A miz-> 50 100 150 200 250 300 350 400 450 30.80 31.00 31.20 31.40

11797.D GCMS0520.M Fri May 24 08:34:46 2002 Page 2

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