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GC/MS analysis results for sample AD22552, Sept 2001

Machine-extracted title · confidence 100%

Laboratory report documenting GC/MS analysis of sample AD22552 conducted on September 27, 2001, identifying unknown compounds.

NYC-WTC_000087068–000087087

Folder label: “508 Scan 9/18/01 9/27/01

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Scanned page image, NYC-WTC_000087085
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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\SEP2601\22552.D Vial: 6 Acq On : 26 Sep 2001 4:15 pm Operator: GALOS Sample : GC/MS unknown Inst : GC/MS Ins Mise Multiplr; 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP072501.M (RTE Integrator) Title : 208 625/TCLP calibration table 7/25/01 Cl IS 5 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 9 Dotriacontane Concentration Rank 4 R.T. EstConc Area Relative to ISTD R.T. 33.87 1.02 ng/uL 75068 Chrysene-dl2 33.31 Hit# of 5 Tentative ID MW MolForm CAS# Qual Qz Dotriacontane 451 C32H66 000544-85-4 83 Tricosane 324 C23H48 000638-67-5 83 3 Triacontane 422 C30H62 000638-68-6 83 4 Tetratetracontane 619 C44H90 007098-22-8 83 Abundance Scan 3166 (33.868 min): 22552.D (-) m/z 57.10 100.00% 5(7

5000 85

207 33.60 33.80 34.00 34.20 m/z43.10 72.41%

_1 TiZz-> 50 100 150 200 250 300 350 400 450 Abundance #74490: Dotriacontane 43

71 5000 33.60 33.80 34.00 34.20 m/z 71705 58.11% 1 I 97 ,,127 155 183 I.... 379 407 450 50 100 150 200 250 300 350 400 450 ^bundance #73318: Tricosane 43

T 71 33.60 33.80 34.00 34.20 5000 m/z 85.05 40.04%

IT-?' I ■ 324 .............. T)/2-> 50 100 150 200 250 300 350 400 450 Abundance #55461: Triacontane 43 _3a6g_33,80_3400^420_ m/z 41.10 26.59% 71 5000

239 267 379 422 ■nZz-> 50 100 150 200 250 300 350 400 450 33.60 33.80 34.00 34.20

22552.D NP072501.M Mon Oct 01 13:03:23 2001 Page 9

NYC-WTC_000087085

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NYC-WTC_000087085Source: NYC Law Department, mirrored locally

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