GCMS results log, sample AD26991, Dec 11 2001

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Library Search Compound Report

Data File C:\HPCHEM\l\DATA\DEC0601\26991.D Vial: 17 Acq On 7 Dec 2001 12 :43 am Operator: GALOS Sample gc/ms unknown Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 10 Dotriacontane Concentration Rank 9

R.T. EstConc Area Relative to ISTD R.T.

35.55 0.47 ng/uL 114035 Perylene-dl2 37.27

Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 Dotriacontane 451 C32H66 000544-85-4 2 10-Methylnonadecane 282 C20H42 000000-00-0 3 Pentatriacontane 493 C35H72 000630-07-9 4 Tetratetracontane 619 C44H90 007098-22-8 Abundance Scan 3349 (35.550 min): 26991.0 (-) m/z 57.10 100.00%| 57

5000 85 A,M IEEt/ M — 35.20 35.40 35.60 35.80 i 207 m/ z 43..10 67.43% m/z-> 50 100 150 200 250 300 350 400 450 Abundance #74491: Dotriacontane 7

5000- 85 -A-AM444 AAMMewAp 35.20 35.40 35.60 35.80 m/ Z 71.05 52.21% 1113 141 196 281 422rr—ii 450 I • ' ' L ii—||ir—i | r m/z-> 50 100 150 200 250 300 350 400 450 Abundance #39858: 10-Methylnonadecane I 57 hA ■ । ■ ■ ■ 1 । 35.20 35.40 35.60 35.80 • ' i ' 85 5000-

m/z--> Abundance 50

57 1113 100 154

150 200 250 300 #58743: Pentatriacontane 350 400 450 ■ T" ‘ I" -TT-r-j-r-r 35.20 35.40 35.60 35.80 TT

m/ Z 55.10 33.93% 5000 85

1 113 1141 ■ 169 197 225 TIr m/z-> 50 100 150 200 250 300 350 400 450 35.20 35.40 35.60 35.80

26991.D NP112701.M Tue Dec 11 14:54:40 2001 Page 10

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