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GC/MS analysis results for sample AD22552, Sept 2001

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Laboratory report documenting GC/MS analysis of sample AD22552 conducted on September 27, 2001, identifying unknown compounds.

NYC-WTC_000087068–000087087

Folder label: “508 Scan 9/18/01 9/27/01

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\l\DATA\SEP2601\22552.D Vial: 6 Acq On : 26 Sep 2001 4:15 pm Operator: GALOS Sample : GC/MS unknown Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP072501.M (RTE Integrator) Title : 208 625/TCLP calibration table 7/25/01 Cl IS 5 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 8 Heptadecane Concentration Rank 5 R.T. EstConc Area Relative to ISTD R.T. 32.91 0.96 ng/uL 70644 Chrysene-dl2 33.31 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Heptai cane 240 C17H36 000629-78-7 50 2 Hexa"' lecane 226 C16H34 000544-76-3 42 3 H /kane, 3,3-dimethyl- 114 C8H18 000563-16-6 38 4 iecane, 2,2,7-trimethyl- 184 C13H28 062237-99-4 36 ^^ndance Scan 3062 (32.914 min): 22552,D (-) m/z 57.10 100.00% 57

5000 43 71 ......1^,., ... 85

99 32.60 32.80 33.00 33.20 I. 1 1 ' I ‘ ‘ I ' m/z 43.10 70.00% Ti/z-> 20 40 60 80 100 120 140 160 180 200 220 240 Abundance #71191: Heptadecane 517 43 71 5000 85 32.60 32.80 33W 33.20 m/z7170559.68% 99, t13 127 ,141, , , 240 Tlfe-> 20 40 (60 80 100 120 140 160 180 200 220 240 Abundance #70789: Hexadecane 57 43 32.60 32.80 33,00 33.20 71 m/z85.05 40.82% 5000 I 85

I I il , . ....... . ^6 Tl/z-> 20 40 60 80 100 120 140 160 180 200 220 240 Abundance #64223: Hexane, 3,3-dimethyl- 43 32.60 32.80 33.00 33.20 m/z41.10 23.53% 57 71 85 5000

27

n^-> 20 40 uu 60 80 99 100 120 140 160 180 200 220 240 32.60 32.80 33.00 33.20

22552.D NP072501.M Mon bet 01 13:03:22 2001 Page 8

NYC-WTC_000087084

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NYC-WTC_000087084Source: NYC Law Department, mirrored locally

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